GCMS analysis results, sample AE09394, May 8, 2002

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Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09394 with unknown compounds and surrogate data from May 8, 2002.

NYC-WTC_000043097–000043111

Folder label: “GCMS X 4/18/02 A 5/1/02”

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0102\9394.D Vial: 12 Acq On 1 May 2002 6:12 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.80 1.47 ug/1 122569 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 (80 2 Benzeneethanam/ne, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 3 N- (Trifluoracetyl) -0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 28 4 N-(Trifluoroacetyl) 0,0 ,0‘‘-tris(t 481 C19H34F3NO4Si3 000000-00-0 28 Abundance 7 Scan 1065 (14.802 min): 9394.D (-) m/z 73.10 100.00% 73

5000 267 355 । i i i i । i i i / । T I i i [ i i i i । i r

45 14.40 14.60 14.80 15.00 15.20 108 154 193 223 323 , , 1 I , ii । । iii । r i ) ।। ’i iii । । ' T “I I III I I I ill [ I I _I I" I I I I I I 1 I I I I < I m/z 267.05 25.85% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 J "id 14.40 14.60 14.80 15.00 15.20 m/z 355.10 23.78% ■ ■ ■ I 1 . . . 207 ... 323 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 ................../ .................... I III I I I I 1 I I I I I I I I I I I I I I

14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 8.63%

45 | 208 251 281 386 458 548 1 1 'i 1 1 i ’ ■ ‘ ' i 1 1 ' ' i ‘ ' i ''1 ‘ 1 i ' ■ 1 1 i ' 1 **I*IIII‘I11“‘ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O',O”-tris(trimethylsilyl)epin ...................... \........................ 73 14.40 14,60 14.80 15.00 15.20 355 m/ Z 74.10 8.37%

5000

45 | 1 140 184 281 480 .................. /.................... tf3 - V i- । । । । । । । “i / । । । । । । । 'i । । । । । i । । । । 1 1 1 i ' 1 1 ' i ' । ii । । [ । n । । । । i i ।" i' r' r i । i i m/z-> 50 100 150 200 250 300 350 400 450 500 550 | 14.40 14.60 14.80 15.00 15.20

9394.D GCMS0501.M Thu May 02 12:03:09 2002 Page 3

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GCMS analysis results, sample AE09395, May 9, 2002 · Box DEP Box 25

NYC-WTC_000043112

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996