Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09396 with unknown compounds and surrogate data from May 9, 2002.
NYC-WTC_000043124–000043134Folder label: “GCMS X 4/18/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY0102\9396.D Vial: 14 Acq On 1 May 2002 8:04 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.81 0.93 ug/1 80967 Naphthalene-d8 15.84
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 80 2 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 40 3 N-(Trif luoroa/cetyl)-N, O, 0 ' , 01 ' - tetr 553 C22H42F3NO4Si4 000000-00-0 38 4 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 1066 (14.808 min): 9396.D (-) m/z 73.05 100.00% 73
5000 267 355 i 1 ■ 1 1 i ■ 1 ' ' i 45 14.40 14.60 14.80 15.00 15.20 133 162 193 223 i 323 i um ' i 1 1 11 No)")’ i ti 1 I I I l l' ' I" I !1 I I IT I I l I I I I I I I I I I I I I m/z 355.10 30.37% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
5000 267 355 .. n.. 14.40 14.60 14.80 15.00 15.20 m/z 267.05 29.96% 207 ... 323. 14 r i ' ■ i ■ • ■ ‘ i ' ' ' ' i ’ ' ■ ■ ■ m/z- > 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 1..( 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.10 11.10% 44 , 147 193 267294 i .“l i J I I I I I I I k1 1 I I I 1 I I I 1 I I I I- 1 I I"T I"' I I' I J" "I ■ 1
miz->_______ 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O''-tetrakis(trimethylsi 73 14.40 14.60 14.80 15.00 15.20 m/z 74.10 8.16% 355 5000
45 i „ 147 193 267 538 1 1 । 1 1 I I । 1 | । । | i r Cl ‘ [ I I I I | i i f i i ii i । I I I 1] i i ‘ i ‘ 1 r 1 i 1 1 ' ' i ' 1 i ' ■ ■ ' । 1 1 1 1 ।' m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
9396.D GCMS0501.M Thu May 02 12:03:48 2002 Page 3
NYC-WTC_000043133
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NYC-WTC_000043112
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043058
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09391 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043590
Summary of GC/MS analytical results for sample AE09674 processed on May 10, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043186
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09450 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043735
Analytical report for sample AE09581 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043632
Laboratory report documenting GCMS analysis of sample AE09098 conducted on May 10, 2002, including detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043609
Summary of GC/MS analytical results for sample AE08952 processed on April 29, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043600
Summary of GC/MS analytical results for sample AE09675 processed on May 10, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023335
Laboratory report showing GC/MS analysis results for sample AE09518 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023372
Laboratory report showing GC/MS analysis results for sample AE09446 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023292
Laboratory report showing GCMS analysis of sample AE08487 conducted on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023255
Laboratory report documenting the detection of unknown compounds and surrogate recovery in sample AE08271 on May 16, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000043032
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 18 and May 1, 2002.
Filed in the same folder
NYC-WTC_000043033
Three-page laboratory record detailing GCMS method parameters including drip rates and volumes for samples analyzed in May 2002.
Filed in the same folder
NYC-WTC_000043036
Ten-page laboratory report showing GCMS blank analysis results for volatile organic compounds with values below detection limits.
Filed in the same folder
NYC-WTC_000043046
Four-page document containing GCMS calibration data and response factors for various chemical compounds analyzed on May 1, 2002.
Filed in the same folder
NYC-WTC_000043050
Eight-page laboratory report showing GCMS reference analysis results for volatile organic compounds analyzed on May 1, 2002.
Filed in the same folder