GCMS analysis results for sample AE04036, Mar 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAR2202\4036.D Vial: 44 Acq On : 24 Mar 2002 12:32 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.86 1.74 ug/1 257751 Naphthalene-d8 15.90

Hit# Of 5 Tentative ID MW Mol Form- CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 N-(Trifluorodcetyl)-N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 37 3 N-(Trifluoroacetyl)-0,0',O''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 1070 (14.865 min): 4036.D (-) m/ z 73.00 100.00% 73

5000 267 355

—.... 4..... — 45 14.60 14.80 15.00 15.20 i । 119 154 193 223 1 323 I 1 r i ’ ‘ — i 1 1 i'' 1 + — 1 1IIddu,aETETTTTTTTT m/ z 267.00 47.46% miz->_ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1 14.60 14.80 15.00 15.20 m/ z 3 55.05 46.69% i 207 323 j m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance - 73 ................... ............. ................... 355 14.60 14.80 15.00 15.20 5000 m/ z 3 56.05 17.34%

45 147 193 267 538 ■ ■ । 1 1 ■ ■ i • ■ ■ ■ i ■ ■ ■ < i ■ ■ ■ > i ■ • ■ ■ । ■ IT । -i । > 1 । । । > i । । i । ' । । । ■ ■ i 1 ’ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluoroacetyij-b,d,,6"-tris(trimethylsilyijno —........... ------ 73 14.60 14.80 15.00 15.20 355 m/z 268.00 12.28% 5000

45 L , 120 147 193 265 481 — । i ' 1 1 1 i 1 1 1 1 i ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

4036.D GCMS0308.M Tue Mar 26 10:49:29 2002 Page 1

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