NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration data for TCLP analysis, May 2002
Machine-extracted title · confidence 90%Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
NYC-WTC_000023122–000023129Folder label: “GCMS X 5/8/02 A 5/9/02”
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NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAYO302\9574.D Vial: 47 4 Acq On 5 May 2002 1:05 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.
14.80 3.19 ug/1 290840 Naphthalene-d8 15.82
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzoic acid, 2,4-bis (trimethylsil 370 C16H30O4Si3 010586-16-0 38 3 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 4 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 37 Abundance Scan 1065 (14.797 min): 9574.D (-) m/ z 73.10 100.00%| 73
5000 267 355 mmm... .. 45 14.40 14.60 14.80 15.00 15.20 108 154 193 223 , 323 - —T I’1 1* 11/ ■ ■ । ' ■ ■ • । 1 ■ ■ ■ । 1 1 ■ ■ । ■ m/z 267.05 34.24% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 14.40 14.60 14.80 15.00 15.20 m/Z 355.10 32.84% ■ ■ ■ i ' ' .2 —I ———323 ————————————— m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73
14.40 14.60 14.80'15.00 15.20 5000 355 m/z 356.10 11.21% 45 133 193 223 281 ————————————————————— mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentaf)uorophenyl)methylene] 73 355 14.40 14.60 14.80 15.00 15.20 m/z 267.95 8.93% 5000
45 | 208 251 281 , , I 386... 458 548 ‘ 'I ' ’ m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
9574.D GCMS0501.M Tue May 07 15:01:07 2002 Page 2
NYC-WTC_000023128
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