GCMS analysis results, sample AE09396, May 9, 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09396 with unknown compounds and surrogate data from May 9, 2002.

NYC-WTC_000043124–000043134

Folder label: “GCMS X 4/18/02 A 5/1/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0102\9396.D Vial: 14 Acq On 1 May 2002 8:04 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.61 2.22 ug/1 152569 1,4-Dichlorobenzene-d4 12.21 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2/86 2 2-Oxo-4-phenyl/6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0-9 3 6,7-Benzo-phenothiazine-5,5-dioxide . 281 C16H11NO2S 000000-00-0 9 4 Benzene, l-pnenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 717 (11.610 min): 9396.D (-) m/z 281.00 100.00% 281

5000

73 133 11.20 11.40 11.60 11.80 12.00 43 59 । 87 103 119 | 147 163 177 193 207 I I I I I 'l l I I I I I I ] 1 I I I I I I I i 'l l I I I I + 235 249 265 1i' r11i1 1 ' 1 i 1 11 ■ i 11 ' ' I — m/z 2 82.00 28.73% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 A I 11 11.20 11.40 11.60 11.80 12.00 TTT

m/z 283.00 18.17% 101 207 73 133 163 177 191 I 235 249 265 ■ ' I 1 ■ ' 1 i ■ ' ' 1 i 1 ' ■ ' i 1 1 1 1 i ‘ 1 ■ 1 i ' 1 T [ I P f । i ' i i i । i T I i ] I — — I i i । 1* i i । i i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 1 i ■ ■ 11.20 11.40 11.60 11.80 12.00 5000 m/z 133.10 11.09%

102 123 141 175 204 247 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 281 L "kid 11.20 11.40 11.60 11.80 12.00 I ' 1 ' 1 I ' '

m/ Z 73.10 8.77%

5000 217 232 102 ns 189 204 „ ll t r-1 n i i | i n i | । । r i । । । । UI । * 1 [ P — I II I I I I1' I I —I I 1"" I I l —r 252264 ........ /rik 1-1 IJ ... ' 1 1 1 ' ' 1 I A m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 11.20 11.40 11.60 11.80 12.00

9396.D GCMS0501.M Thu May 02 12:03:47 2002 Page 2

NYC-WTC_000043132

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000043132Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results, sample AE09395, May 9, 2002 · Box DEP Box 25

NYC-WTC_000043112

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999