GCMS analysis results, sample AE09394, May 8, 2002

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Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09394 with unknown compounds and surrogate data from May 8, 2002.

NYC-WTC_000043097–000043111

Folder label: “GCMS X 4/18/02 A 5/1/02”

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0102\9394.D Vial: 12 Acq On 1 May 2002 6:12 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************* ********************* * ** * * Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.61 2.93 ug/1 192848 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 87 2 2-0xo-4-phe/iyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 Benzene, 1/phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 4 1,3,5,7-Tetraethylbicyclo[3.3.1]tet 310 C8H2205Si4 073420-21-0 9 Abundance Scan 717 (11.613 min): 9394.D (-) m/z 281.00 100.00% 281

5000

43 73 133 59 | 87 103 119, | 147 163 177 191 207 249 265 .. B.. 11.20 11.40 11.60 11.80 12.00 235 I., 0- TTTPTTT I l l-l' l-’<—I I I I I I I I t I i I I I I I I I I I I I I . hjad ‘ 1 i ' 1 1 ’ i 1 11 ‘ I ' 1 11 4— I.. m/z 282.00 28.91% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

/ 5000 T 11.20 11.40 11.60 11.80 12.00 m/z 2 83.00 19.37% 133 207 73 163 177 191 - 235 249 265 I TIPPT 1 1 i 1 ■ ■ ■ । 1 j ■| ■ i ■ ■ ■ ■ । ■ 1 1 11 1 1 ‘ ■ i ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 । 11.20 11.40 11.60 11.80 12.00 5000 m/z 133.10 11.55%

__________________ 102 123 141 175 204 247 ——m——m— a——— -—PDTT—uINuIOROTTTNTRTTTm mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 ........ \......... Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 281 11.20 11.40 11.60 11.80 12.00 rn/z 73.10 8.57%

5000

253 126 203 । 266 ...................... T.................. ,, T224’ 1 1 240 ′ 17141 111’11"/1 111 !11‘+1‘+‘*I/‘‘41‘‘‘1/1.7 1 1 1 ,, li, I , ,1, N AA I 1 1 ' II 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 11.20 11.40 11.60 11.80 12.00

9394.D GCMS0501.M Thu May 02 12:03:08 2002 Page 2

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GCMS analysis results, sample AE09395, May 9, 2002 · Box DEP Box 25

NYC-WTC_000043112

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996