GCMS analysis results, sample AE09394, May 8, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0102\9394.D Vial: 12 Acq On 1 May 2002 6:12 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.19 13.14 ug/1 863646 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 Butane / 58 C4H10 000106-97-8 5 4 Morpholine, 4-methyl-_______________ 101 C5H11NO 000109-02-4 5 Abundance ‘ Scan 343 (8.186 min): 9394.D (-) m/z 43.05 100.00% 43

5000 59

101 7.80 8.00 8.20 8.40 8.60 .............. 38 I ---53 , 67 83 m/z 59.10 44.05% 1 i ■ 1 1 1 i ■ ■ ' ■ i 1 ' 1 1 i 1 1 1 1 i 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 413

5000 । । TddtrU ।_ । । । । । । 11 । । i । । । i r

59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 15.57% 27 101 PT +9— H .......................... 11 83 ' 1 i 1 ■ 1 ■ i ' 1 1 1 I I 1 ■ 1 ■ i 1 1 1 ' i ''' ' 1 i 1 nlz->_______ 10 20 30 40 60 50 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.57%

58 72 100 .................. . , , 38,1 -- ‘ l । ■ 1 ■ । ■ ■ ■ ■ | ■ ■ ■ ■ । ■ n/z->_______ 10 20 30 40 50 60 70 80 90 100 110 Abundance #99: Butane ‘I’’ ■ ■ i 1 1 i ' 1 1 n 1 1 11 i1 1 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.05 7.06% 5000 29

15 58 -। । I । । । । । । । I + | I | I । । 1 I | I I I I | I — I | > I [ I | I I i I | | — । | r । । i i < । । i i i । । i । । । । । 1 m । i 7 rn/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9394.D GCMS0501.M Thu May 02 12:03:08 2002 Page 1

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