Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
NYC-WTC_000043112–000043123Folder label: “GCMS X 4/18/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\l\DATA\MAY0102\9395.D Vial: 13 Acq On 1 May 2002 7:08 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.61 \2.48 ng/1 182920 1,4-Dichlorobenzene-d4 12.21
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2(91 2 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-pnenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 717 (11.612 min): 9395.D (-) m/z 281.00 100.00% 281
5000 .......n....... 11.20 11.40 11.60 11.80 12.00 43 59 73 87 103 119133 147 163 177 191 207 235 2419 265 m/z 2 82.00 28.64% m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
................. \....................... 5000 I I I I I I > I I k I I I I [ t ( I I I I 1
11.20 11.40 11.60 11.80 12.00 m/z 283.00 17.48% 207 73 133 163 177 191 235 249 265 mlz-> > . i . . . . । . . . . । . > ■ . । . . . . । . . . . । . 40 60 80 100 120 140 160 180 200 220 A 240 I. I ' I ' ■ 1 1 1 1 ' 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 ......... M........... ।111111 ■ ■ ■ ।1 ■' ■ । ‘111' 11.20 11.40 11.60 11.80 12.00 5000- m/z 133.10 9.71%
102 123 141 175 204 247 ' ' I 1 ' 1 ' I ' ’ ' ' I 1 ' ' 1 I ... । . i .. i1 । । । I । i | । . ।T •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 1iBit 281 11.20 11.40 11.60 11.80 12.00 m/ Z 73.10 8.69%
5000 217 232
miz-> 102 118 189 204 Dgu । । । । । । 1 । । । । । । । । । ! । i i r-1 । n i । । । । i । । । iL r ।' । 'I । ।"" । r 40 60 80 100 120 140 160 180 200 220 240 260 I 1.1I | i 252264 । i > I l I I i | I I
280 11.20 11.40 11.60 11.80 12.00 A —AAA
9395.D GCMS0501.M Thu May 02 12:03:31 2002 Page 3
NYC-WTC_000043121
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NYC-WTC_000043124
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09396 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043058
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09391 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043186
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09450 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043590
Summary of GC/MS analytical results for sample AE09674 processed on May 10, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045266
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10436 conducted on May 20, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043097
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09394 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043609
Summary of GC/MS analytical results for sample AE08952 processed on April 29, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023372
Laboratory report showing GC/MS analysis results for sample AE09446 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023292
Laboratory report showing GCMS analysis of sample AE08487 conducted on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023335
Laboratory report showing GC/MS analysis results for sample AE09518 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023255
Laboratory report documenting the detection of unknown compounds and surrogate recovery in sample AE08271 on May 16, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000043032
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 18 and May 1, 2002.
Filed in the same folder
NYC-WTC_000043033
Three-page laboratory record detailing GCMS method parameters including drip rates and volumes for samples analyzed in May 2002.
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NYC-WTC_000043036
Ten-page laboratory report showing GCMS blank analysis results for volatile organic compounds with values below detection limits.
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NYC-WTC_000043046
Four-page document containing GCMS calibration data and response factors for various chemical compounds analyzed on May 1, 2002.
Filed in the same folder
NYC-WTC_000043050
Eight-page laboratory report showing GCMS reference analysis results for volatile organic compounds analyzed on May 1, 2002.
Filed in the same folder