GCMS analysis results, sample AE09397, May 9, 2002

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Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09397 with unknown compounds and surrogate data from May 9, 2002.

NYC-WTC_000043135–000043145

Folder label: “GCMS X 4/18/02 A 5/1/02”

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NYC 9/11 Public Portal Document ULULCLy DCC ii L

Data File C:\HPCHEM\1\DATA\MAY0102\9397.D vial: 15 Acq On 1 May 2002 8:58 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.61 1.62 ug/1 114944 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 (87 2 4-Amino-5-(4-acetylphenylazo) benzof 281 C14H11N5O2 000000-00-0 38 3 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 46,7-Benzo-phenothiazine-5,5-dioxide281C16H11NO2S 000000-00-0 9 Abundance Scan 717 (11.612 min): 9397.D (-) m/z 281.00 100.00% 281

5000

11.20 11.40 11.60 11.80 12.00 43 59 73 87 103 119133 147 163 177 191 207 235 249 265 27.57% 11/111)1n 11 j 1 ■' rf ‘111nu).m ri । । i । > i' '| i r i । । * i < I.. i 1 ' 1 ■ I —T m/z 282.00 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

................... । । i ...................... ।I । ‘IBi i i । । i t rqlr । । 5000 11.20 11.40 11.60 11.80 12.00 m/z 283.00 17.77% 133 207 73 m/z—> i ' ' I 1 ’ ■ ■ । ■ > ■ ■ । ■ ■ ■ ‘ i ■ ' 40 60 80 100 120 140 163 177 191 160 180 200 X 220 235240249260265 280 ’ I 1 1 ' ' I ' ' 1 1 i ■ ■ 1 1 I1 1

Abundance #39574: 4-Amino-5-(4-acetylphenylazo)benzofurazan 281 1 .......... 1IT 1 ' 1 ' I ' ' 1 1-1 11.20 11.40 11.60 11.80 12.00 5000 m/Z 133.10 9.68% 116 134 162 77

- 180-194 1 209 238 252 266 . I -J. 1_ - 11_ - I__ _ ■ ■ i ■ ■ 1 ' i ■ । 1 '11 । ■ 11 1 । 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 11.20 11.40 11.60 11.80 12.00 m/ Z 73.10 8.26%

5000

I I J I I I > I I l—I ! J I I 102 I I I I 123 r I I I I I ' 141 i jiii i j । 175 ii 204 2V । । i’r I I I I I I I ' I "I“ I I I I I I I I I 'l I I I I r ......... JAA । । । । i । । । । । । ii । i । li । i d r

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 11.20 11.40 11.60 11.80 12.00

9397 .D GCMS0501.M Thu May 02 12:04:04 2002 Page 2

NYC-WTC_000043143

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NYC-WTC_000043143Source: NYC Law Department, mirrored locally

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