GCMS analysis results, sample AE09397, May 9, 2002

NYC 9/11 Public Portal Document LLJLcLy oCaii topouru ICpUL

Data File C:\HPCHEM\1\DATA\MAY0102\9397.D Vial: 15 Acq On 1 May 2002 8:58 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.18 13.83 ug/1 978688 1,4-Dichlorobenzene-d4 12.21

Hit# of Tentative ID MW MolForm CAS# Qual

1 2 - Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 Butane 58 C4H10 000106-97-8 5 Abundance- Scan 342 (8.175 min): 9397.D (-) m/z 43.05 100.00% 43

5000 59

| | | | | I | ' I r I j i i i i | I I I I | I

101 780 8.00 8.20 8.40 8.60 381 53 , 69 83............. |............. ' 1 I 'I I ' I I I I I 1 I I I I 1 i 1 1'1' 1 1 m/z 59.10 42.94% m/z-> 10 20 30 50 40 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000- ‘II* "I I | I I I I | I I I T | I I I I | T- 59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 15.69% 27 101 -------------- 49 tIH+ — — 83 H m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 । 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 12.93%

58 | 38 I./72 100 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.15%

5000- 15 58 27 ----- I I I : I I I ki1 ' J-1 I l 1”—1 I I-11 I I I I t I I ' t ' 1 1 1 I 1 ' 1 1 I I I ' I I I ‘ I ’ I I 1 ' i 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9397.D GCMS0501.M Thu May 02 12:04:04 2002 Page 1

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