Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.
NYC-WTC_000043146–000043160Folder label: “GCMS X 4/18/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY0102\9398.D Vial: 16 Acq On 1 May 2002 9:54 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.61 4.34 ug/1 265063 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane , octamethyl- 296 C8H24O4Si4 000556-67-2 87/1 2 2-0xo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000 -00-0’-9 3 3,6-Bis (N-dimethylamino) -9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, -phenyl-4- (2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance 7 Scan 717 (11.608 min): 9398.D (-) m/z 2 81.00 100.00% 281
5000
[ ' । । : | । I i I | I 1 I I | I I I I | I I
45 59 73 89 103 119 133 147 163 177 191 207 221 22E 249 265 11.20 11.40 11.60 11.80 12.00 23b |, । i । | T i I i '| i r i"i |' i T i t । T i I i r i i i | 1 'i 1 i i i i i j i rdnpneof I 1 I 1 ' 1 1 I 1 1 ' I ‘ ' 1 ' I — m/z 282.00 28.31%| m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
, ......................... 5000 1 1 1 - ' 1 1 1 1 1 1 I 1 I 11.20 11.40 11.60 11.80 12.00 m/z 283.00 18.36%| 73 133 207 — —] 1 ' 163 177 191 235 249 1265 i ‘ ' 1 ' i r ' ' 1 i ' 1 ■ । 1 1 ■ 11 ■ 1 " ' 1 I ' ' •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 ........ / \......... 11.20 11.40 11.60 11.80 12.00 5000 m/ Z 133.10 10.78%|
102 123 141 175 204 247 ' ' I 1 1 ' 1 1 1 1 1 ' I ' ' ' 1 1 1 ' 1 ' 1 1 1 ' 1 I ' 1 1 ’ | ' 1 1 ' | ' 1 ' itin r i । ■! i । i | i 'i i i । i i i i " m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624:3,6-Bis(N-dimethylamino)-9-ethylcarbazole ___________ \__________ । i । । ' । । i-1 । । । I I i । । r-,i i । i i 281 11.20 11,40 11.60 11.80 12.00 m/z 73.10 8.88%
5000 266
141 250 ..................... | । । । i inny n i i —208 222 237 I । । |' । । r i 1 I 1 k I I I I I ’ I I I I I < I < I I l t I I > I I I I I AA— 11 1 i ' i ' ■ 1 1 i m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 11.20 11.40 11.60 11.80 12.00
9398.D GCMS0501.M Thu May 02 12:04:37 2002 Page 3
NYC-WTC_000043153
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NYC-WTC_000043079
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043726
Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045223
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10432 conducted on May 20, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043058
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09391 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043112
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044723
Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023363
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023148
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023076
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
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NYC-WTC_000043032
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 18 and May 1, 2002.
Filed in the same folder
NYC-WTC_000043033
Three-page laboratory record detailing GCMS method parameters including drip rates and volumes for samples analyzed in May 2002.
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NYC-WTC_000043036
Ten-page laboratory report showing GCMS blank analysis results for volatile organic compounds with values below detection limits.
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NYC-WTC_000043046
Four-page document containing GCMS calibration data and response factors for various chemical compounds analyzed on May 1, 2002.
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NYC-WTC_000043050
Eight-page laboratory report showing GCMS reference analysis results for volatile organic compounds analyzed on May 1, 2002.
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