GCMS calibration table, May 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0102\9398.D Vial: 16 Acq On 1 May 2002 9:54 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.81 3.74 ug/1 287985 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 370 C10H30O5S15 000541-02- 068595-79- 953 7(99 3 Benzeneacetic/acid, .alpha.,4-bis [ ( 326 C15H26O4Si2 055334-40-2 37 4 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 33 Abundance Scan 1066 (14.807 min): 9398.D (-) m/z 73.10 100.00% 73

5000 267 355 I ' 1 ' ' I 1 1 ' ' I

45 14.40 14.60 14.80 15.00 15.20 I 1, 108125 154 177193208223 251 . 323339 111 ■r "Irin i । 'i r i i"| r i r i [ i 'i th [T ri TTTTm । 'i i i r । i 1h i j r F"i i r m/z 267.05 29.63% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 l i i L i । i r । r i i i । kl i i । i r 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 28.35% 191207 323339 ""Tt I' ’ ’' 11 ‘1 11 r ' ■1 r 11 ' i punumreemm VUE m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 I ' ‘ ' I ' ' ' ' I ' ' > ■ i ■ ■

14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 10.35% 5000

45 147 179 356 A 209 237 312 341 I 1 1 1 1 ' ' ' I 1 1 1 1 | ‘111/1 t । । । । । । । । । । T । । । । i ”i i ( Yr" I | I I > r | , I I i | i i il il i i < | i i i i | i T "hut m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #46278: Benzeneacetic acid, .alpha., 4-bis[(trimethylsilyl)o ................. /.................... । 1 1 1 1 । 1 ' 1 1 । ■ 1 ■ i ' ' 1 ■ i 1 1 73 14.40 14.60 14.80 15.00 15.20 267 m/z 74.10 8.36%

5000-

89 151 179 ........ | ................. I i 'r i r i i i i i i 283I 311 I 194.... 237252, I I i i pI ' । । iTn । i । i 1(1 > । । । । n [1 । । । । । [1 । । ' । । । i । । । i ! r । i i i i । i i i i । i r '1 11 11 1 r1 *'' 11 11 1111 1 ' 11 11 11 11'1 i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9398.D GCMS0501.M Thu May 02 12:04:37 2002 Page 4

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