GCMS quantitation results for sample AE04030, March 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAR2202\4030.D Vial: 36 Acq On : 24 Mar 2002 4:37 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.86 0.66 ug/1 105372 Naphthalene-d8 15.90

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 87 2 Benzoic acid, 2-[ (trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 47 3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 32 4 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 32 Abundance Scan 1069 (14.857 min): 4030.D (-) m/z 73.0,0 100.00% 7'3

5000 267 355 _........ 1 1 I111 ‘ 1 1 1 45 14.60 14.80 15.00) 15.20 _ L 111 133 154 17.7193 223 25 1 | 323339 || ‘1’111117'11"1 ■ i"111"1111111 r1 TTTTT '' TTUOTTITTIT ■ ■ ■ 111 । . 1111 •1 i “ ■ ■ ■ 1" 1 “ i11' ■ i m/ z 2 67.00 4 0.13% m/z-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 -....... 267 5000 14.60 14.80 15.00 15.20__ m/z 355.05 33.77% 191207 251 323339 "ItT’1111’1111’1111t11111111111111111/11111111111111111511111111111111111 i11111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 1 / Ho ■ ((t MI ■ yiad . .. 1. m . 73 _.................. • ' I * I 1 1 I 1 ' 1 1 I • ’ 14.60 14.80 15.001 15.20 267 m/z 356.05 13.28% 5000

45 92 135151 175 193 209 233249 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bis[(trimethyisiIyijoxy]-, trimet 73 355 14.60 14.80 15.00 15.20__ m/z 74.00 10.46% 5000

147 267 , 249 m/z-> 47 208 11 " '11 " " i " " i " ‘ ■ i' ■ " i " " i " " i ■ ‘ " ITTTTTTTTTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 —283, .............1370 • I'''11'1111'11111'1 r I 14.60 14.80 15.00 15.20

4030.D GCMS0308.M Tue Mar 26 10:43:55 2002 Page 2

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