NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\1\DATA\MAY0902\8487.D Vial: 12
Acq On : 10 May 2002 1:12 am Operator:
Sample : GC/MS SCAN 5/8 Inst : 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.79 1.99 ug/1 174747 Naphthalene-d8 15.83
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H30O5Si5 000541-02-6 59
2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38
3 Benzoic acid, 2,5-bis (trimethylsilo 370 C16H30O4Si3 003618-20-0 38
4 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37
Abundance Scan 1064 (14.793 min): 8487.D (-) rn/z 73.10 100.00%
73 A
5000
267 355 ..... ... 1
45 14.40 14.60 14.80 15.00 15.20
I I 125 154 193 223 , , 323
1 'I ' ' - 11.T m/z 267.05 30.63%
mz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000
14.40 14.60 14.80 15.00 1520
m/ z 355.10 28.31%
207
——— 1 1 i ' 1 1 1 I1 ' 1 ’ i ■' ■ ■ ' I■
323
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene]
73 355
14.40 14.60 14.80 15.00 1520
5000 m/z 356.10 9.89%
45
‘ I’’
................ 208 251.281 ........ 386... 458 548
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls
B
73 14.40 14.60 14.80 15.00 15.20
355 m/ Z 74.10 8.05%
5000
45
147 179 223, 267 297
' ' i ' ' ' ' i ' ' ' ' i ' ■ ' ' i ' ' ' ‘ I 1 ' ' ' i ' ■ ' ■ i
m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
8487.D GCMS0510.M Fri May 10 13:58:08 2002 Page 2
NYC-WTC_000023300
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