GCMS analysis results, sample AE09395, May 9, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0102\9395.D Vial: 13 Acq On 1 May 2002 7:08 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.80 0.85 ug/1 79854 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83/ 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 43 3 Benzoic acid/ 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 38 4 N-(Trifluoroacetyl)-0,01,011-tris(t 481 C19H34F3NO4Si3 000000-00-0 28 Abundance Scan 1065 (14.801 min): 9395.D (-) m/z 73.05 100.00% 73

5000 267 355 । । । । । । r~i t ‘ T i । । । । । t-1 j i r

45 14.40 14.60 14.80 15.00 15.20 '"17 — III 108 133 154 100011 193 223 251—— 11111111111 323339 |, I '11 1 1 ■'11 1 'l1 1 ' " I 1 1 vv m/z 267.05 25.49% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 22.64%

‘ ‘1‘ i" " r "11' "TTT 191207 r 11' i' " ' I 2511 i11111' 111 323339 11' •'1 i 1 ।1'111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 i 1 1 1 1 i TTT 14.40 14.60 14.80 15.00 15.20 5000 179 267 m/z 74.10 9.14% 356 45 147 209 237 , |, 312 । । 1 nr [Tu । । । । । I I 'I1 I I I I I I I I I I I I I I I I I I I I I ‘ 15 11 i11" i1 " 11'1 " i " 1' i " 111 r 1 ’11 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls । i i I I ] ! I 1 — 1 m I | I i r f | > i

73 14.40 14.60 14.80 15.00 15.20 355 m/z 356.10 8.14%

5000

45 , 147 179 207223 , I'1111'' 111'11 ‘ 111 " 11' ‘ ’ I “ 111 267 297 17Trr । । । । । । । । < । । |-r । । । । । । 11 " 'I । i i r~i । । 17011.......... ....... ।—1 , j—। ] । । । -|—p ! —। 11" " r 1 " i " " i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9395.D GCMS0501.M Thu May 02 12:03:32 2002 Page 4

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