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GCMS analysis results for sample AE08271, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting the detection of unknown compounds and surrogate recovery in sample AE08271 on May 16, 2002.

NYC-WTC_000023255–000023265

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0 902\8271.D Vial: 9 Acq On 9 May 2002 10:13 pm Operator: Sample GC/MS SCAN 5/8 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-dlO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.71 0.44 ug/1 42725 Phenanthrene-dl0 25.57

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 (83 2 Anthracene-d10- 188 C14D10 001719-06-8 72 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 38 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 38 Abundance / Scan 2256 (25.710 min): 8271 .D (-) m/z 188.15 100.00% 188

5000

94 ' ' I ' ' ' ■ I ‘ ' 1 1 I ' 1 1 1 1 1 ' ' 1 I 80

m/z-> —— 42 52 66 PPTTTTTTTTTTTTTTTT 156

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 . I.. m/z 94.10 25,40 25.60 25.80 26.00 19.03% Abundance #19958: Phenanthrene-d10 11®

,.... 5000 25.40 25.60 25.80 26.00 m/z 189.15 17.23% 80 160 66

m/z-> IPIT 40 50 60 70 80 - ...... I*... 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 11® . 4+.. 25.40 25.60 25.80 26.00 5000 m/z 80.10 13.69%

66 80 94 160 - miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 25.40 25.60 25.80 26.00 m/z 184.15 12.18%

5000 143

m/z-> 64 116 130 ■' i ■ " ■ r - —PITP 40 50 89 „lu... 60 70 80 90 100 110 120 130 140 150 160 170 180 190 | IIT 21 25.40 25.60 25.80 26.00

8271.D GCMS0510.M Fri May 10 13:57:17 2002 Page 3

NYC-WTC_000023264

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NYC-WTC_000023264Source: NYC Law Department, mirrored locally

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