Laboratory report documenting the detection of unknown compounds and surrogate recovery in sample AE08271 on May 16, 2002.
NYC-WTC_000023255–000023265Folder label: “GCMS X 5/8/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY0 902\8271.D Vial: 9 Acq On 9 May 2002 10:13 pm Operator: Sample GC/MS SCAN 5/8 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.80 3.55 ug/1 329257 Naphthalene-d8 15.82
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopenta loxane, decamethyl- 370 C10H3005Si5 000541-02-6 83) 2 Phenethyl admine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Noradrenal ine, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzene hanamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 32 Abundance Scan 1065 (14.796 min): 8271.D (-) m/z 73.10 100.00% 73
5000 267 355
45 14.40 14.60 14.80 15.00 15.20 108 133154 193 237, 1 29293 323 — ■ ■ .i i -—.—... . . .L.,—at—4- . ■ " ‘ r * 1 1 11 । ■ m/z 267.05 37.01% mfe-> 50 100 150 200 250 300 350 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 ,..... 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 35.79% ............ 207 J 323 I li m/z-> 50 100 150 200 250 300 350 400 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73
14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.10 12.60% 44
miz-> X TK 50 100 147 150 193 200 250 267 294 300 । 350 400 Abundance #57357: Noradrenaline, tetra-TMS ,1 73 14.40 14.60 14.80 15.00 15.20 m/z 267.95 9.58%
5000 102 355
45 | 147 442 TT IT m/z—> 50 100 150 200 250 300 350 400 14.40 14.60 14.80 15.00 15.20
8271.D GCMS0510.M Fri May 10 13:57:16 2002 Page 2
NYC-WTC_000023263
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NYC-WTC_000023372
Laboratory report showing GC/MS analysis results for sample AE09446 including surrogate recovery data on May 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023335
Laboratory report showing GC/MS analysis results for sample AE09518 including surrogate recovery data on May 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023292
Laboratory report showing GCMS analysis of sample AE08487 conducted on May 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043590
Summary of GC/MS analytical results for sample AE09674 processed on May 10, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043572
Summary of GC/MS analytical results for sample AE09652 processed on May 10, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043124
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09396 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043600
Summary of GC/MS analytical results for sample AE09675 processed on May 10, 2002, including surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045279
GCMS analytical report for sample AE10437 showing unknown compounds and surrogate recovery data from May 20, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044847
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10166 on May 10, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045214
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10431 conducted on May 20, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045238
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10433 conducted on May 20, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043112
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000022961
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000022962
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder
NYC-WTC_000022965
Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.
Filed in the same folder
NYC-WTC_000022990
Laboratory report documenting GCMS calibration verification analysis conducted on May 14, 2002.
Filed in the same folder
NYC-WTC_000022994
Laboratory report of GCMS reference standard analysis conducted on May 14, 2002, showing recovery percentages.
Filed in the same folder