GCMS blank analysis results for volatile organics, May 2002

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Laboratory report of gas chromatography mass spectrometry blank analysis for volatile organic compounds conducted on May 9, 2002.

NYC-WTC_000023207–000023215

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0902\LB.D Vial: 3 Acq On 9 May 2002 4:15 pm Operator: Sample GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.79 1.39 ug/1 121949 Naphthalene-d8 15.83

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Cyclopent iloxane, decamethyl- 370 C10H3005Si5 000541-02-6 (8 2 Benzenee .anamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 43 3 Pheneth amine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 40 4 Benzen thanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 1064 (14.793 min): LB.D (-) m/z 73.10 100.00% 73

5000 267 355 ------------------------------- 45 14,40 14.60 14.80 15.00 15.20 1, 108 133 154 177193 223 251 t 323339 I, Th1—100——‘0———/m/m—HTuEETTTEI 111111 pi । '1111"" 11 m/z 267.05 32.64% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 -----— 5000 ’ I ' ' 14.40 14.60 14.80 15.00 15.20 m/z 355.10 28.38% , . 191207 251 | 323339 T‘n——0‘1—011—00*n1—0n0‘0‘01—0T‘r " i ■ " 11 " ■ ■ 'i " T’’ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 — 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 10.44% 267

mfz-> 4 40 44

60 151 179194209 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 250

Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 14.40 14.60 14.80 15.00 15.20 m/z 74.10 8.93%

5000 355 44

m/z—> 88 -n-pI ' ' i ' ' “ | । । । । । 130147 । 193 267 . i | i , , . । . , , . । . . , , । . . , , । . , . . । i, । 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 294 । ,,, ,( ,, , ,। , 4 ------- 14.40 14.60 14.80 15.00 15.20

LB.D GCMS0510.M Fri May 10 13:59:33 2002 Page 2

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