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GCMS analysis results for sample AE09446, May 2002

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Laboratory report showing GC/MS analysis results for sample AE09446 including surrogate recovery data on May 16, 2002.

NYC-WTC_000023372–000023382

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023380
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAY0902\9446.D Vial: 13 Acq On : 10 May 2002 2:11 am Operator: Sample : GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.80 2.50 ug/1 207258 Naphthalene-d8 15.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclope: as il oxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 3,4-Dih droxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 Abundance 7 Scan 1065 (14.799 min): 9446.D (-) m/ z 73.10 100.00% 73

5000 267 355 .............. . ....................... 14.40 14.60 14.80 15.00 15.20 45 I, 111 ' I 108 133154 191 223 „ 1 323l... m/z 267.05 38.74% m/z-> 50 100 150 200 250 300 350 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 38.12% ............ 207 । 323 I R '' 1 ' 1 1 1 1 ' 1 1 miz-> 50 100 150 200 250 300 350 400 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73

14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 14.06% 5000 179 356 45 147 I, 209 237, 312 ............... 'i 1 m/z-> 50 100 150 200 250 300 350 400 Abundance #57357: Noradrenaline, tetra-TMS 73 14.40 14.60 14.80 15.00 15.20 m/z 267.95 9.92%

5000 102 355

45 1 147 442 Tl " i m/z—> 50 100 150 200 250 300 350 400 14.40 14.60 14.80 15.00 15.20

9446.D GCMS0510.M Fri May 10 13:58:28 2002 Page 2

NYC-WTC_000023380

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NYC-WTC_000023380Source: NYC Law Department, mirrored locally

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