NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\l\DATA\MAY0902\9446.D Vial: 13
Acq On : 10 May 2002 2:11 am Operator:
Sample : GC/MS SCAN 5/8 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.80 2.50 ug/1 207258 Naphthalene-d8 15.83
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclope: as il oxane, decamethyl- 370 C10H3005Si5 000541-02-6 64
2 3,4-Dih droxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43
3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37
4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37
Abundance 7 Scan 1065 (14.799 min): 9446.D (-) m/ z 73.10 100.00%
73
5000 267 355
.............. . .......................
14.40 14.60 14.80 15.00 15.20
45
I, 111 '
I 108 133154 191 223 „ 1 323l... m/z 267.05 38.74%
m/z-> 50 100 150 200 250 300 350 400
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000
14.40 14.60 14.80 15.00 15.20
m/z 355.10 38.12%
............ 207 । 323 I
R '' 1 ' 1 1 1 1 ' 1 1
miz-> 50 100 150 200 250 300 350 400
Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)-
73
14.40 14.60 14.80 15.00 15.20
267 m/z 356.10 14.06%
5000 179
356
45 147
I, 209 237, 312 ...............
'i 1
m/z-> 50 100 150 200 250 300 350 400
Abundance #57357: Noradrenaline, tetra-TMS
73 14.40 14.60 14.80 15.00 15.20
m/z 267.95 9.92%
5000 102 355
45
1 147 442
Tl " i
m/z—> 50 100 150 200 250 300 350 400 14.40 14.60 14.80 15.00 15.20
9446.D GCMS0510.M Fri May 10 13:58:28 2002 Page 2
NYC-WTC_000023380
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