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GCMS Sample AE03387 Report, March 12 2002

Machine-extracted title · confidence 95%

Initial GCMS analysis report for sample AE03387 conducted by analyst DLV on March 12, 2002.

NYC-WTC_000006282–000006291

Folder label: “GCMS X 2/14/02 A 2/23/02

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Scanned page image, NYC-WTC_000006290
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NYC 9/11 Public Portal Document

Data File : C: \HPCHEM\ 1 \DATA\ FEB2 102\3387.D Vial: 49 Acq On : 23 Feb 2002 4:23 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.88 0.22 ug/1 21538 Phenant hr'ene - dl 0 25.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 90 2 Anthracene-diO- 188 C14D10 001719-06-8 87 3 1,4-Naphthalenedione, 5-hydroxy-2-m 188 C11H803 000481-42-5 47 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 9 Abundance Scan 2269 (25.877min): 3387.D (-) ]m/z188.10100.00% 188

5000 - 80 94 158

m/z-> 30 40 PPP 40 50 66 phapuuile 111 " I " I l i ■ ’ ■ ■ i | 1’3 60 70 80 90 100 110 120 130 140 150 160 170 180 190 111111—17 25.60 25.80 26.00 26.20 m/ z 158.05 17.49% Abundance #19958: Phenanthrene-d10 188

-- 5000 25.60 25.80 26.00 26.20 m/z 160.05 15.55% 66 80 94 0mmm**Dmm 160 ,, m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 7 • 188 11/ — . 25.60 25.80 26.00 26.20 5000 m/ z 94.00 15.12%

— 80 94 160 66 m/z-> 30 Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #19854: 1,4-Naphthalenedione, 5-hydroxy-2-methyl- 188 .... A...... . 25.60 25.80 26.00 26.20 m/z 79.95 14.47% 5000 63 92 131 120 51 77 160 173 103 —mPT 11 *1' 11 I...... ------ TT-ph-n-p-T "Il " I “ 1' I ■1 I ■11' 111 IIr m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3387.D GCMS0208.M Fri Mar 08 09:44:26 2002 Page 2

NYC-WTC_000006290

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NYC-WTC_000006290Source: NYC Law Department, mirrored locally

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