Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09391 with unknown compounds and surrogate data from May 8, 2002.
NYC-WTC_000043058–000043069Folder label: “GCMS X 4/18/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\l\DATA\MAY0102\9391.D Vial: 10 Acq On 1 May 2002 4:20 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************** * ***************************************** Peak Number 4 Anthracene-d10- Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
25.72 0.45 ug/1 37257 Phenanthrene-dl0 25.58
Hit# of Tentative ID 5 MW MolForm CAS# Qual 1 Anthracene 10- 7 188 C14D10 001719-06-8/80 2 Phenanthrene-dl0 188 C14D10 001517-22-2 80 3 -(4-Tolyl/-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 4H-Pyridp[1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 28 Abundance Scan 2257 (25.719 min): 9391 .D (-) m/z 188.15 100.00% 188
5000 ......... /......................... 80 94 1 I |”T I 1 | 1 I VI | Illi | I 11 1 [
44 == 66 160 — 25.40 25.60 25.80 26.00 "TTT 36111/777,111117 + - ■ I | I I >! | I I | I I I - I I I I | I ■ I I - , Il | , — m/ z 94.10 19.77% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188
I — i । 4 — । r । । । । । i । । । । । r 5000 25.40 25.60 25.80 26.00 m/z 189.15 18.00% __ 80 94 1 60 1
m/z-> 66 1111 11111.11111. j 111 11111111111111111111111.111.... ।.... ।.... ।.. 111..
30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 IU .... All.. Abundance #19958: Phenanthrene-d10 188 ................. ..................... I I I I I I I I I I I < I I I I I I I I I I I
25.40 25.60 25.80 26.00 5000 m/ z 80.00 17.98%
80 94 160 66 r m I । • I . I | I ... | I| m/z-> . ।... • i.... ।..'' । . 1. ।. 30 40 50 60 70 A ।... • i... . । 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one 188 25.40 25.60 25.80 26.00 91 m/z 44.05 14.62% wNwWyw 105 5000 119 65
m/z~> 30 40 50 60 478 TT 146 1 i I । । । । । i n Tm । ir rl > । i r i i | i i < ■ | i i i i | i i 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 1 i 1 1 1 1 i
9391.D GCMS0501.M Thu May 02 12:02:04 2002 Page 4
NYC-WTC_000043068
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NYC-WTC_000043112
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043124
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09396 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043186
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09450 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043590
Summary of GC/MS analytical results for sample AE09674 processed on May 10, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043097
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09394 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043609
Summary of GC/MS analytical results for sample AE08952 processed on April 29, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023372
Laboratory report showing GC/MS analysis results for sample AE09446 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023292
Laboratory report showing GCMS analysis of sample AE08487 conducted on May 16, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023255
Laboratory report documenting the detection of unknown compounds and surrogate recovery in sample AE08271 on May 16, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023345
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09518 analyzed in May 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000043032
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 18 and May 1, 2002.
Filed in the same folder
NYC-WTC_000043033
Three-page laboratory record detailing GCMS method parameters including drip rates and volumes for samples analyzed in May 2002.
Filed in the same folder
NYC-WTC_000043036
Ten-page laboratory report showing GCMS blank analysis results for volatile organic compounds with values below detection limits.
Filed in the same folder
NYC-WTC_000043046
Four-page document containing GCMS calibration data and response factors for various chemical compounds analyzed on May 1, 2002.
Filed in the same folder
NYC-WTC_000043050
Eight-page laboratory report showing GCMS reference analysis results for volatile organic compounds analyzed on May 1, 2002.
Filed in the same folder