GCMS analysis results for unknown compounds, sample AE10165, May 2002

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Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10165 on May 10, 2002.

NYC-WTC_000044836–000044846

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0602\10165.D Vial: 13 Acq On 8 May 2002 5:35 am Operator: Sample GC/MS SCAN 4/29 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 25.72 0.45 ug/1 34023 Phenanthrene-dl0 25.58 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dl 0 - /S 188 C14D10 001719-06-8 74 2 Phenanthrene-dl0Z Z 188 C14D10 001517-22-2 74 3 -(4-Tolyl) -3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 4H-Pyri,do [1,2-a] pyrimidin-4-one , 3- 188 C11H12N2O 057773-19-0 28 Abundance Scan 2256 (25.716 min): 10165.D (-) m/ z 188.15 100.00% 188

5000

94 ........../...................... i i । । i । । ।g । t i । i । । । [ । । । । । 80 40 49 66 156 25.40 25.60 25.80 26.00 11" 1111. ।111'' | 1111 1111 [ I 11 r 11 r '1 ‘ i 1’1’11’11’1 | 1 1 [ I | I I i f | ! > > i | ! Li 1 1 ■ i'111111 m/z 94.10 19.56% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

1 1 | 1 I A s i T i | I I 1 I | I I I I |" 5000- 25.40 25.60 25.80 26.00 m/z 189.15 16.49% 80 94 160 66 111111111 > 111 ■ 111111111111111111111111111111111111 rrr 11 m 111 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 / r 1 i 1 1 ‘ ' i 1 1 i 1 1 ' ■ i ■ ' ' 1 i 25.40 25.60 25.80 26.00 5000 m/z 80.05 14.06%

94 80 160 66 m/z-> — I ‘' 11' 1' 11111 ( HH P+ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ...... W... Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one ...... /I -.................. r i | i । i i [ i । । i |i i I i ] I I । । । 188 25.40 25.60 25.80 26.00 91 m/z 184.15 13.66% 105 5000 119 65 ..............1... 78., | 146 • i111 ■ i' n ' r 111111111 ■1111'1' ' I 111 ' 11 'I I I I I I 1 I 1 I 1 I I I I I ' I iI r I I I I ( I I I I ■ I ( j ■ I I I I I I ITT ..... n.............. m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25,40 25.60 25.80 26.00

10165.D GCMS0507.M Thu May 09 11:14:02 2002 Page 3

NYC-WTC_000044845

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NYC-WTC_000044845Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE10159, May 2002 · Box DEP Box 25

NYC-WTC_000044804

Laboratory report documenting GCMS analysis of sample AE10159 conducted on May 10, 2002.

1 shared topics · Same agency, volume and box · similarity 0.999