GCMS calibration table for TCLP analysis, February 2002

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Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

NYC-WTC_000052644–000052652

Folder label: “GCMS X 1/15/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1402\1046.D Vial: 9 Acq On : 14 Feb 2002 5:49 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************************************ * * *** * * * * Peak Number 3 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.30 4.25 ug/1 266685 Perylene-dl2 38.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, bis (2- ethylhexyl) 426 C26H50O4 000122-62-3 52 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 25 3 2,4,6(1H,3H,5 )-Pyrimidinetrione, 5 240 C12H20N2O3 051209-93-9 25 4 Butyl citrate 360 C18H3207 000077-94-1 17 Abundance.............. (... Scan 3404 (36.296 min): 1046.D (-) m/z 185.10100.00% 185

5000 70 43

125 139 166 203 268282 297 315 36.00 36.20 36.40 36.60 . । ji a i. ' i ' ' ' ■ I ' ' ' 1 I ' ' ' Trtl 1 । ' । | r I 1 1 > ' i > ■ 1 r' i ' ■ ‘ । 1 m/z 57.00 60.49% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abu de neo #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000 ______ ) _ T' ' 71 112 36.00 36.20 36.40 36.60 m/z 70.10 39.69% 24 9 | 125 143 166 296 316 203 i ' ' ' ■ iTIFrtmpurr i । rI 1 ' ' 1 I 1 mz- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 2687: rope 57 70 --------- 36.00 36.20 36.40 36.60 5000 112 m/z 43.05 34.05% 83

42 98 199 217 ’11111 1’ C 1 " 11 1 " I i ' 1 ' ' i ' ' ' ' i 1 1 1 ' i' 1 ' 1 I ‘ 1 1 ' i ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 1 Mem ?, 1 . Abund #31909: 2I4,6(1H,3H,5H)-Pyrimidinetrione. 5,5-diethyl-1-(1- T—I 1—T ■ . । 185 36.00 36.20 36.40 36.60 m/ z 55.00 33.82% 5000 211 70 54 | 96 114 155168 ........ | TMT 1 140 | 225 240 m/z-> T........ ’IEETTT 40 | ’EtrttttrtrrT 60 80 '1 1 1 i" I 1 1 1 1 1 11 ' 1 1 100 120 140 160 180 200 220 240 260 280 300 320 I ' ■ ■ 1 i ' ' i 1 ' 1 1 i /1 mmo । 36.00 36.20 36.40 36.60

1046.D GCMS0308.M Thu Mar 14 15:30:45 2002 Page 3

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GCMS calibration table for TCLP analysis, Feb 2002 · Box DEP Box 28

NYC-WTC_000052884

Technical document listing calibration standards and response factors for gas chromatography-mass spectrometry analysis of TCLP samples in February 2002.

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