GCMS analysis results for sample AD30251, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2701\30251.D Vial: 8 Acq On : 27 Dec 2001 6:58 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Decanedioic acid, bis(2-ethylh Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.58 1.20 ug/1 211275 Perylene-d12 37.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 58 2 2,4,6(1H,3H,5H)-Pyrimidinetrione, 5 240 C12H20N2O3 051209-93-9 17 3 Butyl citrate 360 C18H3207 000077-94-1 16 4 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 14 Abundance Scan 3326 (35.579 mln): 30251 .D (-) m/z 185.10 100.00% 185 57 5000 112 147 83 221 T-YT-m-r-rr-r • ■ I • 281 355

miz-> — 3 444+444 166 TTH „2047 pm-pT 40 60 80 100120140160180200220240260280300320340360380400420 I 429 m/z 35.20 35.40 35.60 35.80 36.00 56.95 65.34% Abundance #55661: Decanedioic add, bis(2-ethylhexyl) ester 185

5000 57 A MAAA MMAPWA P YR 112 35.20 35.40 35.60 35.80 36.00 83 m/z 73.00 56.34% 143 166 203 298316 *T ITT ——————— m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 ................. '........................ Abundance #31909: 2.4 6(1H.3H.5H)-Pyrimidinetrione, 5.5-diethyl-1-1- 185

35.20 35.40 35.60 35.80 36.00 5000 211 70 96 . | 96114 TWLTgpmmme)mpe]pm]paaaamaT, 155 , ; 240 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance> #50331: Butyl citrate ....... , Ma , A 185 35.20 35.40 35.60 35.80 36.00 129 m/z 71.10 39.59% 5000

57 259 87 111 157 Bam0unu 213 [ .......................... TIpnumt —n9——m"“mITuIIT mpm-q- -A--A—4A miz-> 40 60 80 100120140160180200220240260280300320340360380400420 35.20 35.40 35.60 35.80 36.00

30251.D GCMS1126.M Wed Jan 02 10:38:57 2002 Page 9

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