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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031155
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DECO401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 35.59 42.31 ug/l 9712380 Perylene-d12 37.13

Hit# of 5 Tentative ID MW MolForm CAS# Qu

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H5004 000122-62-3 2 [1,1'-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 3 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO 000000-00-0 17 4 Pyridine, 4-[4-metho hen l]- 185 C12H11NO 000000-00-0 17 scan 3327 (35.590 min): 26205.D (-) m z 185.10 100.00% 1

57 5000 112 83 143 1 35.20 35.40 35.60 35.80 36.00 0 221240 268 297316 355 401 429 m/z 56.95 50 23% ritz-> 40 60 80 100120140160180 200220240260280300320340360380400420 ¼bundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 1

5000 57 • 112 35.20 35.40 35.60 35.80 36.00 m/z 70.00 34.62% 83 143 166 298 -> 40 60 80 100120140160180 200220240260280300320340360380400420 thundance #19199: [1,1'-Biphenyl]-4-ol, 3-amino- 1 I 1 1 1 1 1 1 1 1

35.20 35.40 35.60 35.80 36.00 500o m/z 71.00 33.86% 156 128

-> 40 60 80 100120140160180200220240260280300320340360380400420 Jundance #19197: Pyridine, 4[4methoxyphenyl]- 15 35.20 35.40 35.60 35.80 36.00 m/z 112.10 29.75%

5000 142 115 63 89

n/z-> 40 60 80 100120140160180200220240260280300320340360380400420 35.20 35.40 35.60 35.80 36.00

26205.D NP112601.M The Dec 04 15:59:10 2001 Page 18

NYC-WTC 000031155

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NYC-WTC_000031155Source: NYC Law Department, mirrored locally

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