NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68
Acq On 4 Dec 2001 10:25 am Operator: 209 GALOS
Sample : 11/2 gc/ms Inst GC/MS 209
.:
Misc Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 17 Mercaptoacetic acid, bis(trime Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
34.39 1.38 ug/l 381144 Chrysene-d12 33.04
Hit# of 5 Tentative ID MW MolForm CAS# Qua].
--------------- -----------------------------------------------------
1 Mercaptoace is acid, bis(trimethyls 236 C8H2002SSi2 006398-62-5 23
2 1,1,1,5,7; ,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 17
3 3-Isopro xy-I,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 12
4 Benzoic acid, 2,6-bis[(trimeth lsil 370 C16H3004S13 003782-85-2 i0
ndance Scan 3196 (34.387 min): 26205.D (-) m z 73. 00 100. 00%
147
5000
221
281 35̀5
429 34.00 34.20 34.40 34.60 34.80
45 117 191 249 327 401 m/z 147.00 57.83%
-> 50 100 150 200 250 300 350 400 450 500 550
bundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)-
147
-r fl - r1tyr1
5000
34.00 34.20 34.40 34.60 34.80
221 m/z 221.05 36.70%
45
104 11
-> 50' 100 150 250 300 350 400 450 500 550
Ibundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-b18(trimethyisiloxy)t
34.00 34.20 34.40 34.60 34.80
147
m/z 354.95 22.50%
5000 267
429
207
1 1 1 , 1 11 1 1 1 , , ,, ,, i l , ,
50 100 150 200 250 300 350 400 450 500 550
bundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5tris(fim
34.00 34.20 34.40 34.60 34.80
m/z 281.00 19.70%
5000
147
221 281 327 415 519 561
I I I 1 I I I I I I I '
n/i-> 50 100 150 200 250 300 350 400 450 500 550 34.00 34.20 34.40 34.60 34.80
26205.D NP112601.M Tue Dec 04 15:59:08 2001 Page 17
NYC-WTC 000031154
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