GCMS analysis results for sample AD28428, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28428.D Vial: 28 Acq On : 29 Nov 2001 2:34 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 38.03 0.66 ug/1 70568 Perylene-dl2 37.12 Hit# Of 5 Tentati ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1<1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 Mercaptoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 25 3 Butanoic acid, 3-methyl-3-[(trimeth 262 CllH26O3Si2 055124-90-8 10 4 Trisiloxane, 1,1,1, 5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 10 Abundance Scan 3593 (38.026 min): 28428.D (-) m/z 73.00 100.00% 73 147

5000 221 281 355 _J _ -44--—— — 193 — — — 1 327,.....‘2 I 110/0/*............ | I I T I | II 37.60 37.80 38.00 38.20 38.40 m/z 147.00 82.55% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyI-3,5,5-tris(trim 73

5000 147 37.60 37.80 38.00 38.20 38.40 m/z 221.05 54.88% 221 281 29= 415 519 561 mlz-> ■ ■ । ■ ■ ■ ■ । ■ ■ 1 • । ■ 50 100 150 ..... I...... ..... 200 250 300 350 400 450 1 ■ ■ r ■ ■ ■ ■ ! ■ • ■ ■ । ‘' i' ■ 500 550 Abundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)- 73 147 37.60 37.80 38.00 38.20 38.40 5000 m/z 281.00 30.78% 221 w/ miz-> 1 45

50 104 193..... ..................... ■ TT ■ • • r T ’ ’ I ' f ' I ' • '" I ' ’ ' ' 1 ' ' ’ ' I ' ' ’ ' I ' ' ' ' I ' ' ’ ’ I ' ' 100 150 200 250 300 350 400 450 500 550 Abundance #36157: Butanoic acid, 3-methyl-3-I(trimethylsilyl)oxy}-, t T T 73 131 37.60 37.80 38.00 38.20 38.40 m/z 207.00 28.48% 5000 MAMWWwoA 247

m/z—> 47 | 1 1 p 1 50 | 4 100 15.. 150 200 250 300 350 400 450 500 550 37.60 37.80 38.00 38.20 38.40

28428.D GCMS1126.M Fri Nov 30 13:14:57 2001 Page 2

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