GCMS analysis results for sample AD28428, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28428.D Vial: 28 Acq On : 29 Nov 2001 2:34 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.50 ug/1 114919 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-l,2//3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 42 3 Benzofuran/ 7-chloro- 152 C8H5C10 024410-55-7 9 4 4-Amino-2/chlorobenzonitrile 152 C7H5C1N21 ____ 020925-27-3 9 Abundance Scan 710 (11.559 min): 28428.D (-) m/z 149.90 100.00% 150

5000 115

52 78 11 20 1140 11.60 11.80 ' +++11 ' — 38 1, , 63 . 87 .... - 1— m/z 151.85 ' ' I ’ ----- 64.79% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 11 iO

5000 115 TTTImunn—T TIT । । । I । 78 11.20 11.40 11.60 11.80 52 m/z 115.00 42.67%

mlz—> 30 35 ■ ■ i 1 ■ ' ■ i ' ' ' • i 40 50 '' I' ■1 ■ i ■' 60 70 80 .... L.. 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 11.20 11.40 11.60 11.80.. 5000 52 78 m/z 52.00 19.17%

mz-> 30 35 I ■ ■ i ■ ■ ■ ■ । 40 ■ i 50 • ■ r ■ ■ ■ ■ l < । 60 70 7... 1.. . i ■'1 • i'' ’ ’ । • ■' ■ । ■ ■1 ■ t ■ ■1111111111 80 90 100 110 120 130 140 150 160 Abundance #10136: Benzofuran, 7-chloro- 1!i2 11.20 11.40 11.60 11.80 m/z 78.05 . 18.71% 5000 89

35 49 73 125 ■ i 1 ■ ■ ■ i ■ ■1 ''i 1 p•.......... T I ' ' ' ’ I '' ' ’ I' ' ’ ' I ' ■ I ' m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 1140 11:60 11.80 1

28428.D GCMS1126.M Fri Nov 30 13:14:55 2001 Page 1

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