Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
NYC-WTC_000034402–000034414Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV2901\28428.D Vial: 28 Acq On : 29 Nov 2001 2:34 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopropanamine, N-methyl-l-p Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 39.59 0.87 ug/1 93423 Perylene-dl2 37.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopropanamine, N-methyl-1-phenyl 147 C10H13N 056771-48-3 27 2 Mercaptoacetier acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 25 3 l,l,l,5,7,7,/-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 4 1,2-Bis(triMethylsiloxy)ethane 206 C8H2202Si2 007381-30-8 16 Abundance Scan 3763 (39.586 min): 28428.D (-) m/z 73.00 100.00%| 73 147
221 5000 281 355
J 401 429 39.20 39.40 39.60 39.80 40.00 39 -H— 96 117. .... Tn- TITTTTTUUEETETTT 191 253 mmm i mmmmTT m/z 147.00 87.31% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #9103: Cyclopropanamine, N-methyl-1 -phenyl- 147
5000 1 I" 1 —AA 39.20 39.40 39.60 39.80 40.00 42 | 64 92 120 TTTTTTT Tr 1‘‘7T‘0211l‘‘ITITT‘T‘ITT "I ' H < | i i I I | I । I I | I I . I | i I i I J I mlz-> 40 60 80 100120140160180 2CX)220 240 260280300 320340360 380400 420 Abundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)- 73 147 • i ■ • ■ ■ i ■ < 39 20 39.40 39.60 39.80 40.00 | 5000 m/z 281.00 __ 36.63% 221 193
miz—> 104 TTT mlr ■ ■ । ■ 1111 >. । . TTPTTTTTg 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 39.20 39.40 39.60 39.80 40.00 m/z 355.05 27.09 147 5000 267 355 429 45 207
m/z—> "'I'"' mmk ..4. . 40 60 80 100120140160180200220240260280300320340360380400420 ■pTrrpTTT i" " i" " i ■" ■ i' 1’11 • • i • • 39.20 39.40 39.60 39.80 40.00
28428.D GCMS1126.M Fri Nov 30 13:15:00 2001 Page 3
NYC-WTC_00003441 1
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NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034819
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033789
Analytical commentary for sample AD28151 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033954
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28229 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder