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GCMS analysis results for sample AD24219, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24219 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068037–000068054

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24218.D Vial: 5 Acq On : 1 Nov 2001 6:55 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L Peak Number 6 Mercaptoacetic acid, bis(trime Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 39.63 0.68 ug/1 87143 Perylene-dl2 37.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Mercaptoacj^ic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 32 2 3,7-Dio; 2,8-disilanonane, 2,2,8,8 220 C9H24O2Si2 017887-80-8 27 3 3,6-Dio;^-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 17 4 Ethan^loic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 17 Abundance Scan 3768 (39.634 min); 24218.0 (-) m/z 73.00 100.00% 75 147 221 5000

43 39.40 39.60 39.80 40.00 m/z 147.0074764% n/z-> 40 60 80 1001201401601802002202 0260280300320340360380400420 Abundance #30949: Mercaptoacetic add. bis(trimethylsilyl)- 7(3 147

5000 -........... 39.40 39.60 39.80 40.00 221 m/z 220.9552.88%

nfe-> fikbundance Xi 193 I pTXrpTTTp^TTpTTTJTTTTpTTTp^ 40 60 80 100120140160180200220240260280300320340360380400420 #70531:3,7-Dioxa-2,8-disilanonane, 2,2.8,8-tetramethyl- 147 7“ ^ 39.40 39.60 39.80 40.00 5000 m/z 281.00 24.51%

A 73 115 177 205 Tife-> 40 60 80 100120140160180200220240260280300320340360380400420 vH/vVwy Abundance #41682:3.6-Dioxa-2,4,5,7-tetrasilaoctane, 2.2,4.4,5,5.7,7- T T T 147 2!1 39.40 39.60 39.80 40.00 m/z 354.95 2^737% 73 5000 191 117 279 L ■p I p-rTTpTTT^TTTTpTTTJTTTTJTTT^^

Tnfe-> 40 60 80 100120140160180200220240260280300320340360380400420 39.40 39.60 39.80 40.00

24218.D NP103001.M Tue Nov 06 11:48:41 2001 Page 6

NYC-WTC_000068050

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NYC-WTC_000068050Source: NYC Law Department, mirrored locally

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