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GCMS analysis results for sample AD24219, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24219 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068037–000068054

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\NOV0101\24218.D Vial: 5 Acq On 1 Nov 2001 6:55 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.53 ug/1 78993 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Die orobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzeni l,2,3,4-d4-, 5, 6-dichloro- 150 C6C.12D4 002199-69-1 25 3 Benza lehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 ((3- hoxyphenyl) -1-methanol_______ 152 C9H12O2 000000-00-0 9 ^undance Scan 712 (11.579 min); 24218.D (-) m/z 149.90 100.00% 1!i0 (1

5000 T^^-n-r-r-j-r 115 52 78 ‘ I ‘ ‘ ‘ I ’ ‘ ‘ r' 36 45 87 1120 11.40 11.60 11.80 12.00 I I I I ' I '"l ■ !'■ ■ I'l'i! I .......................................................... m/z 151.90 68.57% ttZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundance #9593; 1,4-Dichlorobenzene-d4 liO

5000 115 ..... 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 38.91% 35 87___________ ' I ‘ ‘' 1' ... ‘ ‘ I ‘ ‘ ‘ ‘ I •' ‘ ' I' ‘ TiZz-> 30 40 50 «) 70 80 90 100 110 120 130 140 150 160 Abundance #8592; Benzene-1,2,3,4-d4-, 5.6-dichloro- l40

115 11.20 11.40 11.60 11.80 12.00 5000- 52 78 m/z 77.95 19.93%

35 87 I I ' 1''' • I' ' I ‘‘ I' T I'' ‘ * I Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 1$2 1120 11.40 11.60 11.80 12.00 m/z 52.00 17798% 106 5000 53 81

Tife-> 30 40 50 60 70 80 n+r 90 92 T 100 110 ux 122

120 130 136 ■ 1 • • ■ • I • ■ • > 1 140 150 160 ' ' I ' 11 11'40 'i?60 iS izob

24218.D NP103001.M Tue Nov 06 11:48:38 2001 Page 5

NYC-WTC_000068049

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NYC-WTC_000068049Source: NYC Law Department, mirrored locally

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