GCMS analysis report, sample AD22558, October 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\22558.D Vial: 3 Acq On : 17 Oct 2001 3:08 pm Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.52 ug/1 49440 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 Tentati ID MW MolForm CAS# Qual 1 1,4-Dichlorobenz^e-d4 150 C6C12D4 003855-82-1 59 2 Benzene-1,2,3,4/a4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 Benzaldehyde, >2-hydroxy-3-methoxy­ 152 C8H8O3 000148-53-8 10 4 2-Methyl-6- irroaniline 152 C7H8N2O2 000570-24-1 10 Wjundance Scan 717 (11.625 min): 22558.D (-) m/z 149.90 100.00% 1ii0

50)0 115 52 78

nZz-> 40 .. I,, 111'111 1111

30 40 50 60 I.. 1 uU 70 80 90 100 110 120 130 I'' ‘ ‘ I 140 150 160 11.20 11.40 11.60 11.80 12.00 m/z 152.00 66.16% Mjunttence #9593:1,4-Dichlorobenzene-ci4 liiO

5000 115 I ' ■ " I " ' ■ P' 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 34.96% 35 TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, S.&dichloro- 1$0

115 5000 52 78 m/z77.95 21.32%

35 87

nfe-> 30 I

40 50 I ' I ' ' ' ' 1 ' * ' ’ I ' ' ' ’ I ' 60 70 80 90 100 110 120 130 A T 140 150 160 ^bundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- T T T 1!i2 11.20 11.40 11.60 11,80 12.00 m/z52.00 18.11% 106 5000 53 81

122 ‘ I ' ‘ ' I ' ‘ ‘ ‘ I I 111 ■ I ■ I' • I' I • • ■ 111 • 136 ■ I < • • 111 • • ‘ 1 I I Yt 1 1 I I i-i 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

22558.D NP101901.M Tue Oct 23 15:08:24 2001 Page 6

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