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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031156
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 19 1-Monolinoleoylglycerol trimet Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 36.73 1.07 ug/1 245675 Perylene-d12 37.13

Hit# of 5 Tenta ve ID MW MolForm CAS# Qual ------------------- ------------------------------------------------- 1 1-Monolinoleoy lycerol trimethylsi 498 C27H54O4Si2 054284-45-6 33 2 Tris(trimethy silyl)borate 278 C9H27BO3Si3 004325-85-3 16 3 1,1,1,5,7,7 -Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 4 Trisiloxa . 1.1.1.5.5.5-hexamethvl 384 C12H36O4Si5 003555-47-3 12 ¼bundance scan 3451 (36.728 min): 26205.D (-) m z 73. 00 100. 00%

147 5000 221 281 355 40 96117 191 253 327 401 429 36'40 36'60 36.80 37'00 m/z 146.95 63.46% rift-> 50 100 150 200 250 300 350 400 450 undance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether

207 5000 147 36.40 36.60 36.80 37.00 34 103 281 m/z 221.05 38.74%

rift-> ,1, 50 100 150 200 250 300 350 395

400 450 482

¼bundance #39028: Tris(trimethylslyl)borate 221

36.40 36.60 36.80 37.00 m/z 281.00 26.21% 263 133 175

rift-> 50 100 150 200 250 300 350 400 450 undance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 3 36.40 36.60 36.80 37.00 m/z 354.95 20.70% 147 5000 267 355 429

II 45 207

rift-> 50 100 150 200 250 300 350 400 450 36.40 36.60 36.80 37.00

26205.D NP112601.M The Dec 04 15:59:13 2001 Page 19

NYC-WTC 000031156

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NYC-WTC_000031156Source: NYC Law Department, mirrored locally

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