GCMS comments for sample AD28901, Dec 17 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0 601\28901.D Vial: 38 Acq On 7 Dec 2001 11:48 am Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Monolinoleoylglycerol trimet Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 35.56 5.60 ug/1 1461690 Perylene-dl2 37.11 Hit# of 5 Tentatiye ID MW MolForm CAS# Qual 1 1-Monolinoleoylg] cerol trimethylsi 498 C27H54O4Si2 054284-45-6 23 2 Tris (trimethylsilyl) borate 278 C9H27BO3Si3 004325-85-3 12 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 10 4 N-(Trifluor^acetyl)-0,0*,OI1-tris(t 481 C19H34F3NO4Si3 000000-00-0 10 Abundance Scan 3324 (35.563 mln): 28901 .D (-) m/z 72.95 100.00%

X i 73

147 5000 221 185 281 355 ri r f >

m/z-> 41 50 112 t - ■■ 100 150 — 4249,4 200 250 —24401’2 300 350 400 450 35.20 35.40 35.60 35.80 m/z 146.95 ........ ........... 58.87% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 T | J i I 4 | T TT T, I • I i | I 1 18| * 35.20 35.40 35.60 35.80 34 103 281 m/z 221.05 39.37% I 395 _ iI > ■ ‘ I ' ' ' ' I ‘ ‘ ’ • I ‘ ' ■ 1 1 1 r ‘ ' 1 1 1 — — ---------- -r-r-[-i—■—482 r-r miz-> 50 100 150 200 250 300 350 400 450 Abundance #39028: Tris(trimethylslylborate 73 221 • i • ■ -PPIPI 1 ‘ 1’ 35.20 35.40 35.60 35.80 5000 m/z 185.10 27.67% 263 133 175 ------------ miz-> 50 100 150 200 250 300 350 400 450 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls ’I T T ' 73 35.20 35.40 35.60 35.80 355 m/z 281.00 22.24% 5000 45 1 ,147 179 223 267 397 • > • 1 * r- । riii TT > -==-===PR-IP==PP m/z—> 50 100 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80

28901.D GCMS1126.M Tue Dec 11 16:08:19 2001 Page 3

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