GCMS analysis results for sample AD29964, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\29964.D Vial: 18 Acq On 19 Dec 2001 9:41 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************** ** * * ******************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.57 19.58 ug/1 3366890 Perylene-dl2 37.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 90 2 [1,11-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 27 3 Octane, 2,5-dimethyl- 142 C10H22 015869-89-3 22 4 Octane, l^'-oxybis- ________________ 242 C16H340 000629-82-3 14 Abundance • Scan 3325 (35.572 min): 29964.D (-) am/ z 185.10 100.00% 185

57 5000 - 112 41 F l ' , f' l t ' * ' • 1 * 143 166 35.20 35.40 35.60 35.80 36.00 203 223 240 268 297 315 369 TTn Tr NTTmipTTT m/z 57.00 59.42% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000- 57 TT TT 112 35.20 35.40 35.60 35.80 36.00 83 m/z " 41.00% 143 166 203 298 316 i ■ ■ " i' ■'1 r TVIU TBIT 11'' ■ i TTTTTTTTTTTTTTTITTI miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #19199: [1.1-Biphenyl)-4-ol, 3-amino- 185 TT "b" 35.20 35.40 35.60 35.80 36.00 5000- m/z " 38.51%

113 139 156 11' " i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #66225: Octane, 2,5-dimethyl- "T 1 1 i ■ ' ' 1 i 1 57 35.20 35.40 35.60 35.80 36.00 m/z 43.00 32.51% 5000

27 1 .1 199 142 1‘‘E‘100—E11TTT“TTTTCTTETET i" " I ‘TET‘ETTUTTTTTTT‘TTETITTTTII‘‘‘I T jT r-r-pn-AIB——n——)r m/z—> 20 40 60 80 1 00 120 140 160 180 200 220 240 260 280 300 320 340 360 35.20 35.40 35.60 35.80 36.00

29964.D GCMS1126.M Tue Jan 15 15:29:47 2002 Page 2

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