DEP GCMS unknown compounds report, Mar 2002

NYC 9/11 Public Portal Document

.Data File : C:\HPCHEM\1\DATA\FEB2502\1802 .D Vial: 28 Acq On : 26 Feb 2002 4:31 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 MisC : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Propanedioic acid, hexyl-, die Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

33.41 0.60 ug/1 39363 Chrysene-dl2 33.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 37 2 3-Ethyl-3-hexene 112 C8H16 016789-51-8 27 3 1,2-Cyclopentanedione, 3-methyl- 112 C6H802 000765-70-8 22 4 2-Nonenal, (E)- 140 C9H160 018829-56-6 22 Abundance Scan 3090 (33.407 min): 1802.D(-) । m/ z 57.00.. 100.00% 57 71 112 43 5000- 83 0 97 157 239 256 ................................ 207 ........ । , , I1, , 33.00 33.20 33.40 33.60 33.80 I 1 1 ' 1 1 1 ' 1 ii m/z 112.10 76.38% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70

5000 ....... W... , 83 112 33.00 33.20 33.40 33.60 33.80 m/z 71.10 70.76%

m/z-> 20 an . 42

40 60 i ■ ■ [ ‘ i 80 98 100 120 140 160 180 199 200 217 220 240 260 Abundance 55

33.00 33.20 33.40 33.60 33.80 5000 83 m/z 70.10 69.78% 112 42 69 97 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #2500: 1,2-Cyclopentanedione, 3-methyl- 112 33.00 33.20 33.40 33.60 33.80 m/ z 43.05 66.47% 5000 55 69 83 27 42 97 i ■ ' ■ ■ i ' ■ i ■ ' 1 I ' ' ' ■ i 1 ' ' ‘ i ' ■ ■ ■ i ' ' ' ' i ' 1 ' ‘ I 1 ' ' ' I ' • ' ' i ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 33.00 33.20 33.40 33.60 33.80

1802.D GCMS0208.M Thu Feb 28 11:52:18 2002 Page 1

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