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GC/MS analysis results for sample AD23082, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23082 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087875–000087892

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087888
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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\OCT0401\23082.D Vial: 2 Acq On 4 Oct 2001 4:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.71 0.76 ug/1 108313 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Dotriacontane 451 C32H66 000544-85-4 91 /Abundance Scan 3123 (33.713 min): 23082.D (-) m/T 57’ 00 16’0.00% £7 71 43 85 5000

‘ ' f

m/z~> UJ 40 •, .x.

(60__ 80 100 120 140 160 ' ■ I .............I ■ ■ ■

180 200 220 240 260 280 300 ■ ■ ■ I ■ 33.40 33.60 33.80 34.00 m/z 71.00 69.62% Abundance #71561: Octadecane

43 71

5000 85 ..A..... 33.40 33.60 33.80 34.00 m/z ^3.05 62.74% T '•‘f 155 . I ' ‘ I ' ' '■* 1 ' ' II 224 2W ni/z-> 40 60 80 100 120. 140 160 180 200 220 240 260 280 300 Abundance #42201; Heneicosane 57 71 : 85 33.40 33.60 33.80 34.00 5000 m/z 85.0,5 49.86% T 113 127 141 155 : H 268 296 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance I #74636; Hexatriacontane ......... ![............ 43 57 33.40 33.60 33.80 34.00 m/z 41.00 23.13% 71 5000 85

97 I II p,. X ................................. . . m/z-> 40 60 80 100 120 140 160 180200220 240 260280 300 33.40 33.60 33.80 34.00

23082.D NP091101.M Tue Oct 09 12:24:12 2001 Page 7

NYC-WTC_000087888

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NYC-WTC_000087888Source: NYC Law Department, mirrored locally

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