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GC/MS analysis results for sample AD22978, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22978 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087754–000087772

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

' Data File C:\HPCHEM\1\DATA\OCTO 3 01\22978.D Vial: 4 Acq On 3 Oct 2001 3:35 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Heptadecane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

32.76 0.62 ug/1 87442 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 9T 2 Octadecane 254 C18H38 000593-45-3 90 3 Pentacosane 352 C25H52 000629-99-2 87 4 Tricosane 324 C23H48 _ ______000638-67-5 87 Abundance Scan 3019 (32.760 min): 22978.D (-) m/z 57.0.0 100.00% 7 43 71 5000 85

• T • ■' I ■ ’ ' ' . . I . > ■ 1 , .

m/z-> IXjb _ 40__ 6g___80 T ' I

100 141 155 ' I ' ’ ' '

120 I ' ' ' I

140 160 180 200 I . 1 183 r 1 I r I I I I 207 I I I

220 240 260 281 280 32.40 32.60 32.80 33.00 m/z 71.00 68.17% Abundance #71193: Heptadecane 57

71 5000- 85 32.40 32.60 32.80 33.00 99 m/z 43.0,5 67.48% A, ....... ..................... •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 ^Abundance #71561; Octadecane 57 i 7.1 ■',^'-'■'■1 I 11 i-pr'Pt I i 32.40 32.60 32.80 33.00 85 5000 m/ Z 85.05 47.74%

li Tn/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #73718; Pentacosane 43 5,7 32.40 32.60 32.80 33.00 m/z 41.0,5 25.62% 71 5000 85

nn/z~> ' I ' ' ' TtJ I, 40 60 80 T. 100 120 140 160 180 200 220 240 260 280 A, f lA ,0/ 32.40 32.60 32.80 33.00

22978.D NP091101.M Tue Oct 09 09:51:34 2001 Page 6

/ NYC-WTC_000087766

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NYC-WTC_000087766Source: NYC Law Department, mirrored locally

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