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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088175
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NYC 9/11 Public Portal Document

Library Search Compound Report •5, Data File C:\HPCHEM\l\DATA\OCT0 901\23264.D Vial: 10 Acq On 9 Oct 2001 10:09 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Heptadecane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.61 0.79 ug/1 178697 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane 240 C17H36 000629-78-7 93v 2 Octadecane 254 C18H38 000593-45-3 93\ 3 Tetracosane 338 C24H50 000646-31-1 91 ) 4 Pentacosane ____________________ 352 C25H52 000629-99-2 91 / Abundance Scan 3221 (34.612 min): 23264.D (-) m/z 56795 TOOTO^ 5(7 43 71 85 5000

a, —|-m-rj-i -IT /| iSt. I . I . , I I 1 I 99 34.20 34.40 34.60 34.80 35.00 . i. ,|J J 41155169183197211 281 240 256 ' I'''' I'''' I' '' I ‘ ra/z 71.00 69.03% n/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #71194; Heptadecane A 4S 5/

5000 71 85 A 34.20 34.40 34.60 34.80 35.00 "m/z 43705 63.09% L. I I T''i^’'27141 155169183 212 240 Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71559: Octadecane 43 5(7

71 34.20 34.40 34.60 34.80 35.00 5000 “m/z 85705 52.96% 85

I I 1191^141155169183 226 254 '' I' ''' I''' 11 ‘' 1'''' 1'''' r''''' 1''''' I'' p-rr-q-m-rj- p 7i/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane L 'T ' I ' ' ' ' I ' 43 57 34.20 34.40 34.60 34.80 35.00 71 ■m/z 41.00 22.32% A 5000- 85

99 ' I''' I I I ‘‘ I il 155169183197 I'''' r ' ' ' I 294 338 I''' ’ I' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23264.D NP091101.M Thu Oct 11 10:53:05 2001 Page 8

NYC-WTC_000088175

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NYC-WTC_000088175Source: NYC Law Department, mirrored locally

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