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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088176
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NYC 9/11 Public Portal Document

Library Search Compound Report J Data File : C:\HPCHEM\1\DATA\OCT0901\23264.D Vial: 10 Acq On : 9 Oct 2001 10:09 pm Operator: 209 GALOS Sample : g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Pentacosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 35.50 0.75 ug/1 155160 Perylene-dl2 37.26 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 91, 2 Heneicosane 296 C21H44 000629-94-7 91 3 Triacontane 422 C30H62 000638-68-6 91 4 Nonacosane ____________________ 408 C29H60 000630-03-5 91 Abundance Scan 3318 (35.502 min): 23264. D (-) m/z 57760 100.00% 5/

5000 85

-r-rTT-TPn | , Pj-i-i i , fi , n 35.20 35.40 35.60 35.80 3! m/z 71.00 69758% Ti/z-> ^bundance 40 60 80 100120140160180 200 220 240260 280 300320340 360380 400420 #73718; Pentacosane A 43

71

35.20 35.40 35.60 35.80 m/z 43.05 58.32% 1 1 , 127 155 183 211 jnVrjiTTT^TT^TpVrrfTTTV^^ I"" I" " I" " r' " I" " I" " I" " I" ‘' I" " I n/z-> 40 60 80 100120140160180 200220 240260 280 300320340 360380 400 420 ^bu^dance #42201: Heneicosane 7

35.20 35.40 35,60 35.80 85 5000 m/z 85.05 47.24%

■m-p-TT n/z-> 40 60 80 100120140160180 200220 240260 280 300 320340 360380 400 420 Abundance #55461: Triacontane " n' " I ........ . 43 35.20 35.40 35.60 35.80 m/z 55.00 23.08% 71 5000

I TI 239 267 JTTTTJTITTpTTTpTTTpTrTprTrqTTTTpTTrpTTrj^^ 379 422 tV2-> 40 60 80 100120140160180 200220240260280300320340360380400420 35.20 35.40 35.60 35.80

23264.D NP091101.M Thu Oct 11 10:53:07 2001 Page 9

NYC-WTC_000088176

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NYC-WTC_000088176Source: NYC Law Department, mirrored locally

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