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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088170
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NYC 9/11 Public Portal Document

Library Search Compound Report 4 Data File C:\HPCHEM\1\DATA\OCT0901\23264.D Vial: 10 '■ Acq On 9 Oct 2001 10:09 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Heptadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 30.70 0.49 ug/1 109937 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 91, 2 Octadecane 254 C18H38 000593-45-3 91 3 Tetracosane 338 C24H50 000646-31-1 90. 4 Nonadecane . 268 C19H40 .000629-92-5 86 Abundance Scan 2795 (30.701 min): 23264.D (-) m/z 57.00 100.00% 57

43 71 85 5000-

A F' ' '

Ti/z-> JUj. 40 60 ■■I' .T 7TrTT*YTTJtVpVrTY-rT-rrp-TTTyTTTTJTT-TTp-TTTpn-TTpn-TT^^ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 _____________ m/z 30.40 30.60 30.80 31.00 71710 71771% Abundance #71193: Heptadecane 5(7'

71 5000 85 30.40 30.60 30.80 31.00 m/z 43.05 61704% 99 J ^P1?7141155169 210 240 . I r. r I I /i . . f. I t ■. I I . rq- I ' p " ' p'' p-iTT-p-rrp-TTTpnrT-rp- •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #71560: Octadecane 43 57

71 30.40 30.60 30.80 31.00 gw 85 m/z 85.05 50.50%

99 I J 169183197 254 pFT-TTY'n-^p-rVTTYTTT-rpT^TprTT^^ J ‘' T'' I p-TT-rp-n-rj m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 4- / \ ' ' ' I 43 5(7 30.40 30.60 30.80 31.00 71 m/z 41.05 28721%

5000 85

99 ll ,i ^27 155169183197 ' I '' J I r ‘' I' 294 p r. , ITT' ' I I ■ . . I . . . . I 338 p-TTp-T aa />a a fvr v\A A AAA^ A

Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

23264.D NP091101.M Thu Oct 11 10:52:54 2001 Page 3

NYC-WTC_000088170

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NYC-WTC_000088170Source: NYC Law Department, mirrored locally

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