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GC/MS analysis results for sample AD23262, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088171
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23264.D Vial: 10 Acq On 9 Oct 2001 10:09 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\bATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.65 0.99 ug/1 223859 Chrysene-dl2 33.13

Hit# of 5 Tent, ive ID MW MolForm CAS# Qual

1 Butyl tetrad< anoate (myristate) 284 C18H36O2: 000000-00-0 72 2 Octadecanoij acid, butyl ester 340 C22H44O2i 000123-95-5 50 3 Cyclobuta. , 1,2-diethyl-, trans- 112 C8H16 019341-98-1 35 4 Cyclope: anecarboxylic acid, 2-amin 129 C6H11NO2 Abundance '' Scan 2898 (31.647 min): 23264.D (-) m/z 56700 100.00% 5^

5000 4 73 129 285 340 31.40 31.60 31.80 32.00 rrfr. m/z SYTOO 49.43% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53

5000 229 .,..,7M_ 31.40 31.60 31.80 32.00

■n/z-> ^Kbundance I'''' I' 20 40 u 73 129 211

I' ’ " I " .. I • I 11 I I rj .y 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73570: Octadecanoic acid, butyl ester 284 ' I I '' ' I'' '' I'' ' ' I m/z 43705 42.56%

53 f-r-i I I'l-i- i>-i -p->-r _3t40_3t60_^t80_JZ00_ 5000 m/z 41705 37773% 285 340

L 129 267

Ti/z-> 20 40 60 Xtxu, I»rrrp- 185 I 241 I I'''' I'''' I'''' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #2701: Cyclobutane, 1,2-diethyl-, trans- 4|1 5lS 31.40 31.60 31.80 32.00 m/z 73.0.0 30.76%

5000

)I j 112 I rn-.-p. . ip . . . I }' •'' I'' " I " *' I I ' " ' I H I I I . I . . j n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23264.D NP091101.M Thu Oct 11 10:52:57 2001 Page 4

NYC-WTC_000088171

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NYC-WTC_000088171Source: NYC Law Department, mirrored locally

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