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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088172
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0901\23264.D Vial; 10 Acq On ; 9 Oct 2001 10;09 pm Operator; 209 GALOS Sample ; g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Tetradecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.74 0.91 ug/1 204966 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Tetradecane 198 C14H30 000629-59-4 9U 2 Heptadecane 240 C17H36 000629-78-7 91> 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90^ 4 Heneicosane __________________ . 296 C21H44 000629-94-7 87 Abundance Scan 2908 (31.738 min): 23264.D (-) m/z 57700 100.00% 57

43 71 85 5000

•n/2-> Abundance '' I' 40 u 60 80 . T, ■ 100 120 140 160 180 #69659: Tetradecane 200 220 ???................... 240 260 280 300 ' ' I ' ' ' ' I 31.40 31.60 31.80 32.00 m/z 71710 A n- 68787%

57 43 71 5000 85 31.40 31.60 31.80 32.00 m/z 43700 64.88% 7 113127141 155168 1?8 n/z-> 40 mLX 60 80 100 120 140 160- 180 200 220 240 260 280 300 Abundance #71193: Heptadecane c 7~

71 31.40 31.60 31.80 32.00 5000 m/z 85.05 49.86% 85 1 99 210 240 I,, ,, I,, .'I,. ???■ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 <\bundance 7 #42196: Heptadecane, 2,6,10,15-tetramethyl- AU 31.40 31.60 31.80 32.00 71 m/z 41.05 24.62% . 5000 85

■n/z-> 40 X ? J^^127y ire, 60 80 100 120 140 160 180 183 200 211 220 240 260 268 280 2^ 300 31.40 31.60 31.80 32.00

23264.D NP091101.M Thu Oct 11 10;52;59 2001 Page 5

NYC-WTC_000088172

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NYC-WTC_000088172Source: NYC Law Department, mirrored locally

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