GCMS analysis comments for sample AD28664, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC04 01\28664.D Vial: 18 Acq On 5 Dec 2001 4:58 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Heptadecane, 2,6,10,15-tetrame Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.67 1.00 ug/1 228093 Chrysene-dl2 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 SI 2 Octadecane 254 C18H38 000593-45-3 bl 3 Pentacosane 352 C25H52 000629-99-2 91 4 Heneicosane 296 C21H44 000629-94-7 90 Abundance Scan 2900 (31.665 mln): 28664.D (-) m/z 57.00 100.00% 57 43 71 85 5000

99 TT TTnrr ' l ' '

mfz~> ■ ■ ■ Th 40 J 60 +4 1.113127 80 141.155 169,183 197210 225 120 140 160 180 100 240 280 300 m/z 43.. 05 200 220 260 31.40 31.60 31.80 32.00 73.57% Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- 57 71 l 5000 85 . ! j I . . , । I I TT | V I I I | < > < t 31.40 31.60 31.80 32.00 m/z 71.00 68.29% • • ■ i • ■ , , L — 113127 141155 . ■ . 183 , , , 211 . .. . miz- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71330: Octadecane 43 57 ■ ■ । •

71 31.40 31.60 31.80 32.00 5000 85 m/z 85.05 51.72%

99 113 17127 141 169 183 197210 254 miz-> ' 40 60 80 100 120 140 160 180 200" 220' 240 260 280 300 Abundance #73718: Pentacosane ‘ ' 1 * 1 • ' I ' ' T ■ ■ i 1 1 43 57 31.40 31.60 31.80 32.00 m/z 41.05 28.60% 71 5000 85

_ 1 L 38 113 127 141 155 169,183 197 211 . ...... - ------- TNTTTTnur miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.40 31.60 31.80 32.00

28664.D GCMS1126.M Fri Dec 07 15:54:04 2001 Page 6

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