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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088169
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23264.D Vial: 10 Acq On : 9 Oct 2001 10:09 pm Operator: 209 GALOS Sample : g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Piperidin-4-carboxylic acid Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.51 1.19 ug/1 268710 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Piperidin-4-carboxylic acid 129 C6H11NO2i 000498-94-2 38 2 1-Hexene, 5-methyl- 98 C7H14 003524-73-0 27 3 1-Hexene, 2-met2^1- 98 C7H14 006094-02-6 27 4 Decane, 2,2,3/rrimethyl-_____________ 184 C13H28 062338-09-4 27 Abundance X Scan 2665 (29.508 min): 23264.D (-) m/z 56.00 100.00% 53

5000 41 129 yr-r ’"I ' ' ' ' I ' ' ' ' I I .bl ®IJ T 1431571711851992^ 29.20 29.40 29.60 29.80 312 . . |T. .'i 11 i\T| .. I'l. I , I I'l 11 I,.I , > I ” ' ■ I ”' ■ I m/z 57700 51767% n/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5228: Piperidin-4-carboxylic acid 5

5000 29.20 29.40 29.60 29.80 30 84 m/z 43.05 36757%

Ti/z-> Abundance Xu 20 40 60 I lx 100 129 -p-m-p-m-j- 80 100 120 140 160 180 200 220 240 260 280 300 #63239:1-Hexene, 5-methyl- 53 / V 41 I' ' ' ' I 29.20 29.40 29.60 29,80 553 m/z 41.05 35.85% 27 I 70 I L I. 98 I’ ' ' ' I ' ' ' ' I ' ' > ' I ' ' ‘ • I ' • ’ ' I ' ' ' < ] ' ' ' ' I ' ’ ' ' I ' ' ' ' I ’ ' ' ' I ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261; 1-Hexene, 2-methyl- 29.20 29.40 29.60 29.80 m/z 73.00 28.52% 41 5000 27 70 98 I Tf-T'' ‘' I X-X I ' ' ' ' I ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23264.D NP091101.M Thu Oct 11 10:52:52 2001 Page 2

NYC-WTC_600b88169

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NYC-WTC_000088169Source: NYC Law Department, mirrored locally

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