NYC 9/11 Public Portal Document
Library Search Compound Report
■ Data File : C:\HPCHEM\1\DATA\OCT1601\23605.D Vial: 12
Acq On : 17 Oct 2001 1:00 am Operator: 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise : Multiplr: 1,00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 6 Piperidin-4-carboxylic acid Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
29.51 2.06 ug/1 218844 Chrysene-dl2 33.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Piperidin/4-carboxylic acid 129 C6H11NO2 000498-94-2 .32
2 1-Rente:ne, 2,4-dimethyl- 98 C7H14 002213-32-3 27
3 1-Hex, e, 2-methyl- 98 C7H14 006094-02-6 27
4 Butyjf hexadecanoate 312 C2 0H40O2 _____ 000000-00-0 25
Abundance Scan 2665 (29.508 min): 23605.D (-) . m/z 56.00 100.00%•
55
553 4’
73
257
129
m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300
X "'i ' ' ' ' I ‘
312
' i ' ' I ' I
29.20 29.40 29.60 29.80
m/z 57.00 51754%
Abundance #5228: Piperidin-4-carboxylic acid
5
5000-
29.20 29.40 29.60 29.80
.30 84
129 m/z 43.05 40.63%
■nfe-> 20
J4
40 60
X I' '' ' I' ' ‘ ’ I ' ' '' I ' ' ‘ ' I' ' '' I' ' ' ' I
80 100 120 140 160 180 200 220 240 260 280 300
Abundance #63263:1-Pentene, 2,4-dimethyl-
53
29.20 29.40 29.60 29.80
4 m/z 41.05 37.96%
5000
27
98
'‘I‘'I''''I‘' I'' ’' r'' ’ I' ’ 1'''' I'''' r ''' I'''' I''' ’ I
n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300
Abundance #1354:1-Hexene, 2-methyl-
53 29.20 29.40 29.60 29.80
m/.z._^73.. 00 31.78% y.
41
5000
-27
Tife-> 20 40
, Il .Il
60
70
80
98
I ' ' ' ' I ' ' ' ' I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I' ' ' ' I''' ' I
100 120 140 160 180 200 220 240 260 280 300
1
29.20 29.40 29.60 29.80
23605.D NP091101.M Thu Oct 18 10:32:31 2001 Page 6
NYC-WTC_0b0d88947
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