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GC/MS analysis results for sample AD23605, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23605 conducted on October 19, 2001.

NYC-WTC_000088935–000088960

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088947
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NYC 9/11 Public Portal Document Library Search Compound Report

■ Data File : C:\HPCHEM\1\DATA\OCT1601\23605.D Vial: 12 Acq On : 17 Oct 2001 1:00 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Piperidin-4-carboxylic acid Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 29.51 2.06 ug/1 218844 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Piperidin/4-carboxylic acid 129 C6H11NO2 000498-94-2 .32 2 1-Rente:ne, 2,4-dimethyl- 98 C7H14 002213-32-3 27 3 1-Hex, e, 2-methyl- 98 C7H14 006094-02-6 27 4 Butyjf hexadecanoate 312 C2 0H40O2 _____ 000000-00-0 25 Abundance Scan 2665 (29.508 min): 23605.D (-) . m/z 56.00 100.00%• 55

553 4’ 73 257 129

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 X "'i ' ' ' ' I ‘ 312 ' i ' ' I ' I 29.20 29.40 29.60 29.80 m/z 57.00 51754% Abundance #5228: Piperidin-4-carboxylic acid 5

5000- 29.20 29.40 29.60 29.80 .30 84 129 m/z 43.05 40.63%

■nfe-> 20 J4 40 60 X I' '' ' I' ' ‘ ’ I ' ' '' I ' ' ‘ ' I' ' '' I' ' ' ' I 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63263:1-Pentene, 2,4-dimethyl- 53

29.20 29.40 29.60 29.80 4 m/z 41.05 37.96% 5000 27

98 '‘I‘'I''''I‘' I'' ’' r'' ’ I' ’ 1'''' I'''' r ''' I'''' I''' ’ I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354:1-Hexene, 2-methyl- 53 29.20 29.40 29.60 29.80 m/.z._^73.. 00 31.78% y. 41 5000

-27

Tife-> 20 40 , Il .Il 60 70

80 98 I ' ' ' ' I ' ' ' ' I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I' ' ' ' I''' ' I 100 120 140 160 180 200 220 240 260 280 300 1 29.20 29.40 29.60 29.80

23605.D NP091101.M Thu Oct 18 10:32:31 2001 Page 6

NYC-WTC_0b0d88947

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NYC-WTC_000088947Source: NYC Law Department, mirrored locally

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