GC/MS analysis results for sample AD23082, Oct 2001

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\OCT0401\23082.D Vial: 2 Acg On : 4 Oct 2001 4:30 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★if

Peak Number 5 Heptadecane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.76 0.58 ug/1 82840 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 2 Hexatriacontane 507 C36H74 000630-06-8 91'- 3 Tetracosane 338 C24H50 000646-31-1 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 ____ 054833-48-6 90'" Abundance Scan 2910 (31.757 min): 23082.D (-) m/ z' 5 7”. 0~0 100 ."O O % 57 71 43 5000 85

'm/z-> Abundance JU 40 , i 1 y\P^27141i55 183 11 n I yr ■ ■ q . । t 11. । f. ■.. ।. i .t 1111 । j 11 11111 11 । 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #71193: Heptadecane p-r-T-q’ 31.40 31.60 31.80 32.00 ' m/z 71.00 74.81%

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71 5000 I 85 31.40 31.60 31.80 32.00 99 m/z 43.05 61.34% I , J ^]3i?^141155169 210 240 ' ' ' ' I ' ' ' ' I ' ‘ fn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Haxatriacontans 43 57

71 31.40 31.60 31.80 32.00 5000 85 m/z 85.05 47.07% I

113127141155169183197211 Tp-m-p- T-r-rTT-p-TTTT-jrTTT-pTTT-ry-rT-T-Tp-TTTp^ p-rT-rpn-r-rj- nn/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane .................. 43 5)7 31.40 31.60 31.80 32.00 71 m/z 41 05 28.18% 5000 85

44-5 1 l| ,| 127 155169183197 ' I''' ' I •' ' ' I'' ' I ■ I' ■ . I.... I. ... I 294 338 I opfA I I I'^r rn/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

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23082.D NP091101.M Tue Oct 09 12:23:55 2001/ Page 5

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