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GC/MS analysis results for sample AD22978, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22978 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087754–000087772

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

' Data File C:\HPCHEM\1\DATA\OCT0 301\22978.D Vial: 4 Acq On 3 Oct 2001 3:35 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Nonadecane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.76 0.62 ug/1 87179 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane 268 C19H40 000629-92-5 91' 2 Hexatriacontane 507 C36H74 000630-06-8 90 3 Heptadecane, 8-methyl- 254 C18H38 013287-23-5 86 4 Octacosane 394 C28H58 __000630-02-4 86 Abundance Scan 2910 (31.759 min): 22978.D (-) m/z 57.00 100.00% 71 43 85

ML 5000

141 155 169 183 31.40 31.60 31.80 32.00 207 200 " 220 ' 240 ' 260 m/z 71.10 75.45% m/z~> 40 60 80 100 120 140 160 180 Abundance :M7469: Nonadecane 57 43 71

5000 85 . .... wA.......... 31.40 31.60 31.80 32.00 99 m/z 43.05 65.14% I ' ' I II 1,1 100 ' 120 140 ' 160 .''Y 180 ' 200 ' ' 220 240 260 ' m/z-> 40 60 80 Abundance #74636: Hexatriacontarie Y 71 31.40 31.60 31.80 32.00 5000 i 85 m/z 85.05 50.85%

^/z-> 40 60 .1 ii T-n-p-r 80 .1 I y100 120__ 140 160 180 200 220 240 260 Abundance 5(7 71 #34816: Heptadecane, 8-methyl- „y,,, 31.40 31.60 31.80 32.00 m/z 41.05 25.54% 85 5000 126 154 y I Il.......... 224 254 Y,. m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 31.40 31.60 31.80 32.00

22978.D NP091101.M Tue Oct 09 09:51:30 2001 Page 5

NYC-WTC_000087765

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NYC-WTC_000087765Source: NYC Law Department, mirrored locally

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