GCMS sample analysis summary, April 29, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0602\8952.D Vial: 9 Acq On 7 May 2002 12:09 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hexadecanoic acid Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

28.08 0.67 ug/1 74669 Phenanthrene-dl0 25.58

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoic acid 256 C16H3202 000057-10-3 38 2 Isopropy Palmitate 298 C19H38O2 000142-91-6 27 3 .alpha.— Galactopyranoside, methyl 194 C7H14O6 003396-99-4 25 4 .alpha/) Glucopyranoside, methyl 3 176 C7H1205 013407-60-8 23 Abundance Scan 2514 (28.081 min): 8952.D (-) m/z 43.10 100.00% 43

60 102 5000 73 256 239 27.80 28.00 28.20 28.40 ii — — J, 1 ,1,1.|1,, l i, T ।. 115 128 157 171 185 213 | i ' m/z 60.00 63.55% m/z--> 40 60 80 100I 120 140 160 180 200 220 240 260 Abundance #35186: Hexadecanoic acid 43 60 73

\ 5000 ' ' 1 1 1 1 '"I Trrr I | I ! I I | I I 27.80 28.00 28.20 28.40 85 97 129 m/ z 41.05 52.11% — 157 III 171 185 213 I 256 1 1 I ' 1 1 1 I ' 1 P I I 1 I • I • i l i • > • I • I > ' I ' • « I I i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #42488: Isopropyl Palmitate 102

27.80 28.00 28.20 28.40 5000 60 m/z 102.15 52.11% 73 129 85 157 ' 1 i 1 ' I I Hill . I' 1 । ■ 1 1 ■ । ■ 1 1 1 i i ' 1 1 1 i 1 ' ’ 1 i 1 ■ ■ ' i ' 1 1 ' i 1 1 257 ' ' i 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #21079: alpha.-D-Galactopyranoside, methyl 63 27.80 28.00 28.20 28.40 m/z 57.10 46.07% 74 5000 31 87 103 116 131 145 163 ■ i ■ ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 27.80 28.00 28.20 28.40

8952.D GCMS0501.M Wed May 08 11:51:57 2002 Page 2

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