GCMS analysis results for sample AE02578, March 2002

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Data File : C:\HPCHEM\1\DATA\MAR1902\2578.D Vial: 27 Acq On : 21 Mar 2002 6:39 am Operator: Sample : gc/ms scan 3/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Heptadecanol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.90 1.03 ug/1 181464 Phenanthrene-dl0 25.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual .A 1 1-Heptadecanol 256 C17H360 001454-85-9 2 3 1-Nonadecanol 1-Octadecanol 284 270 C19H40O C18H380 001454-84-8 000112-92-5 94 33 4 l-Pentadecanol Abundance Scan 2598 (28.899 min): 2578.D () 228 C15H320 m/z 000629-76-5 55. 00.. 10 0.00%theme 91) 43 55 69 83 ft 97

5000 111 - 125

miz-x —41— 40 60 80 4 11 100 120 140 154 168 160 ........................ 224 .......... 180 200 220 240 28.60 28.80 29.00 29.20 m/ z 83.05 95.72% Abundance #35210: 1-Heptadecanol 55 69 83 97 -................. 5000 111 28.60 28.80 29.00 29.20 125 m/ z 43.05 94.70% i 210 238 1 ' i 1 ■ ■ ■ i ■ ■ ■ ■ i ■ i ■ > > ■ । ■ ■ ■ > । ■ i ■ ■ > • i ■ ■ ■ • i ■ ■ > ■ । ■ i m/z-> 40 60 80 120 140 160 180 200 220 240 Abundance — i- 55 22 69 63 97 ' 1 1 1 ' 1 ’ 1 1 1 28.60 28.80 29.00 29.20 5000 m/z 69.10 81.68% 111 31 42 125 _ _ 238 > . ! - r-r - 1r1-TT0mIDTTOIITTOTDTIIIIVCCITITIIIIIIII m/z->__ 40 60 80 100 120 140 160 180 200 220 240 / Abundance #72029: 1-Octadecanol 11I 1 ' I 1 ' 43 55 69 83 28.60 28.80 29.00 29.20 97 m/ z 41.05 77.43% 5000 111 125

■ ' i 1 * ICT r |LL.........................224—252 m/z-> 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20

2578.D GCMS0308.M Thu Mar 21 14:28:03 2002 Page 3

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